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GC/MS analysis results for sample AD23842, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23842 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089385–000089396

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089395
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3001\23842.D Vial: 14 Acq On : 31 Oct 2001 3:12 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ************************************************************************* Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 11.58 0.54 ug/1 109265 1,4-Dichlorobenzene-d4 11.72

Hit# of 5 Tentative ID MW MolForm. CAS# Qual

1 1,4-Dichlorobezfzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-1,2^^Xf4-d4-, 5,6-dichloro- 150 C6C12D4 . 002199-69-1 .38 3 4-Amino-2-(znlorobenzonitrile 152 C7H5C1N2 020925-27-3 10 4 Phenol, i '^methoxy-2,3-dimethyl- 152 C9H12O2. 034883-01-7 9 Abundance Scan 712 (11.578 min): 23842.D {-) m/z 149.90 100.00% 1!i0

5000 115

52 78 40 11 20 11.40 11.60 11.80 12.00 .... m/z 151.90 . 67.68% tVz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 1!i0

5000- 115 - 78 -<11 20 11.40 11.60 11.80 12.00 52 m/z 115.00 . 38.21% 35 ' I ' ' ’ I ' TiZz->‘ 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 1$0 . 11'' •' I ■' • n * ' T'''' I' 115 1120 11.40 11.60 11.80 12.00 5000- 52 78 jiiTz 78.05 20.30%

87 ---- - T j ■ 111 • ■ I'' I ‘ I' ■ 111'''' I'''' I'''' I' ; , ip;;;; TiZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 - 160 Abundance #10110: 4-Annino-2-chlorobenzonitrile 1$2 ' - - “m7z 52.00 18.56%

553

63 90 117 125 I 76 -■ ............ , . q , / , ............... .. l,,,|l,.,|.............. TiZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160- " 11.20 11.40 11.60 11.80 12.00

23842.D NP103001.M Thu Nov 01 14:38:39 2001- Page 3

NYC-WTC_000089395

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NYC-WTC_000089395Source: NYC Law Department, mirrored locally

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