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GCMS analysis results for sample AD24237, Nov 5 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24237 conducted on November 5, 2001, noting unknown compounds.

NYC-WTC_000068085–000068100

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

Library Search Confound Report Data File : C:\HPCHEM\1\DATA\NOV0101\24236.D Vial: 3 Acq On : 1 Nov 2001 2:01 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library ; C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 3.04 ug/1 505505 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 ntative ID MW MolForm CAS# Qual 1 2 - Pent anorafe, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 38 2 5-Hexen^-one 98 C6H10O 000109-49-9 9 3 MorphoMne, 4-methyl- 101 C5HHN0 000109-02-4 9 4 3-Hydroxy-2-pentanone 102 C5H10O2 003142-66-3 9 (Abundance Scan 288 (7.691 min): 24236.D (-) m/z 42.95 100.00% 40

59 5000 101

83 7.40 7.60 7.80 8,00 4^ 71 I I ■ • • ■ I ' ■ • > I • I ■ m/z 59.05 54.81% •nfe-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64275:2-Pentanone, 4-hydroxy-4-methyl-

50001

15 I I 31 I 40

59

83 101 7.40 m/z 100.95 7.60 II ft 7.80 8.00 25.29% ryn—TT-T-y-r-r-T—r-|—r-r-r-r-p TiZz-> 10 20 30 40 60 70 80 90 100 110 (Mjundance #63205:5-Hexen-2-one 40

7.^ 7.ro 7.80 8.00 5000 m/z 5^705^ 17.55% 55 38 50 , I ' ' ' I ' • ' ■ I I I ■ ■ I I I ' I I ■ . 98 • I I • I • ■ I TiZz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1640: Morpholine, 4-methyl- 413 7.40 7.60 7.80 8.00 m/z 41.05 8.04% 5000 101 15 71 ,,,l.... , 56 ‘ I • ■ ■ ■ 1 • • • • I • I • • 1 10 20 30 40 50 60 70 a) 90 100 110 7.40 7.60 7.80 8.00

24236.D NP103001.M Fri Nov 02 11:48:32 2001 Page 5 NYC-WTC_000068097

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NYC-WTC_000068097Source: NYC Law Department, mirrored locally

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