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GCMS analysis results for sample AD24237, Nov 5 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24237 conducted on November 5, 2001, noting unknown compounds.

NYC-WTC_000068085–000068100

Folder label: “GCMS Scan X 10/10/01 An 11/1/01”

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Scanned page image, NYC-WTC_000068096
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NYC 9/11 Public Portal Document

Librairy Search Compound Report Data File S C;\HPCHEM\1\DATA\NOV0101\24236 .D Vial: 3 Acq On : 1 Nov 2001 2:01 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hexanol Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.67 0.52 ug/1 85688 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexan( 102 C6H14O 000626-93-7 78 2 2-Pent .ol, 4-methyl- 102 C6H14O 000108-11-2 64 3 2-Hexi .hoi, (S)- 102 C6H14O 052019-78-0 56 4 2-Bu nol 74 C4H10O 000078-92-2 42 Abundance Scan 177 (6.672 min): 24236.D (-) m/z 44.95 100.00% 4|5

5000 V__ -p-i-PT ( , .TTTTTrri . . , 69 III 51 I 98 6.40 6.60 6.80 7.00 I n 11111111 iTi I p I H111111111111111 fh 111111111111111111 n 11111111111111111 H111111111111111111111 m/z 69.00 15.50% Tlfe-> 10 15 20 25 30 35 40 45 SO 55 60 65 70 75 80 85 re 95 100105 Abundance #63584:2-Hexanol

5000 6.40 6.60 6.80 7.00 69 "mTz 43.95 12.38% 19 27 .................. r,™TTT^™TTTTTTXTTTTTTrT^^

10 15 20 re ot"^"7o"7^"^ ‘^ Abundance #1773; 2-Pentanol, 4-methyl-

6.40 6.60 6.80 7.00 5000 "mTz 41.05 11.82%

69 57 7TTTTp-rrrpTTrp4TTjTTTT^^ I ®7 ,. I,.. 11.,,,I,,,, I,,, 11.1., 111,,I,,,,I.,,, I,,, Tife-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #1769:2-Hexanol, (S)- 4(5 6.40 " are " 6.^ " ^66 " ' m/z 43.05 11.68% 5000

•nfe-> 10 Vs ..... 1^....... 30 re 69 .......................................................................... 55 re re re re 70 75 re re 87 re JVJ r-r-rr-f ■ 6.40 ' " I ‘ ' repPPr 6.60 6.80 TOO

24236.D NP103001.M Fri Nov 02 11:48:30 2001 Page 4 NYC-WTC_000068096

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NYC-WTC_000068096Source: NYC Law Department, mirrored locally

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