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GCMS analysis results for sample AD24237, Nov 5 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24237 conducted on November 5, 2001, noting unknown compounds.

NYC-WTC_000068085–000068100

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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Scanned page image, NYC-WTC_000068095
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0101\24236.D Vial: 3 Acq On : 1 Nov 2001 2:01 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method ; C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.55 0.47 ug/1 78037 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3“Hexanol / 102 C6H14O 000623-37-0 83 2 3-Pentane^ 2-methyl- 102 C6H14O 000565-67-3 38 3 3-Penta^l 88 C5H12O 000584-02-1 36 4 2-Prop^ol, 2-methyl- 74 C4H10O 000075-65-0 36 Abundance Scan 164 (6.553 min): 24236.D (-) m7z 597705 100.00% 55^

73 43 J I ■—p_j—J—J_ 'Py • J »__I_ r~]_ r

<(r39 620 6.40 6.60 6.80 -rrrrf 51 86 -rprTT m/z 54.95 80.52% q • I n ‘i •. • J11111 nZz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 ^bundanc8 #63531:3-Hexanol

55

5000 73 1111 .''i I 6.20 6.40 6,60 6.80 43 ra/z 73.00 41.83% I 11111111111 ■ 1111 ■ 11111111111111111111111111 ■ 111111111111111 69 ■ 111111111111111111111111 1111111 TiZz-> 5 10 15 20 25 30 35 40 45 50 55K)65 70 75 80 85 90 Abundance #1781; 3-Pentanol, 2-melhyk 5)9 . . .........../iS?^.......... » » I • • » • I » I I • I I I I I 1 » I • » 1 » 620 6.40 6.60 6.80 5000- 31 73 m/z 43.00 25.17% 27 55 45 15 69 I" ‘' I T 4 11II11...11.■..I■ ■. 11 nfe-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #851:3-Pentanol 5)9 6.20 6.40 6,60 6.80 "m/z iTToK 24710% 31 5000 27 41 15 jTTTTpTTTTpT-rrpT-TTpTTTyrTTT^^ nfe-> 5 10 15 g) 25 30 35 40 45 50 55 60 65 70 75 80 85 90 6.20 6.40 6.60 6.80

24236.D NP103001.M Fri Nov 02 11:48:29 2001 Page 3 NYC-WTC_000068095

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NYC-WTC_000068095Source: NYC Law Department, mirrored locally

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