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GCMS analysis results for sample AD24334, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of environmental sample AD24334 with detection of unknown compounds.

NYC-WTC_000068240–000068254

Folder label: “508 GCMS Scan X 10/11/01 An 11/2/01

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Scanned page image, NYC-WTC_000068251
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0101\24334.D Vial: 10 Acq On : 1 Nov 2001 11:48 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hexanol Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 6.68 0.58 ug/1 93900 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexani 102 C6H14O 000626-93-7 78 2 2-Pent .ol, 4-methyl- 102 C6H14O 000108-11-2 64 3 2-But .ol 74 C4H10O 000078-92-2 45 4 2-Hl nol, (R) - 102 C6H14O 026549-24-6 43 Abundance Scan 178 (6.676 min): 24334.D (-) m/z 44795 100-00%

5000

—' ' ' ' T . ■'1 . I . , , . I , . . . 69 6.40 6.60 6.80 7.00 39| Il 55 ..... I.............. ................. 101 tTnTTT.,|HrTTTT T m/z 69.00 13.44% Tife-> Abundance 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105

45 #63584:2-HexanoI ft 5000 ......... 6.40 6.60 6.80 7.00 69 ra/z 41.00 13.12% .tit.. ............ ..I I II 1.1. ...| I III I.... I.. .i|. ..l|. I,. I. .1. |....1.1.11.,,,I. •nfz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 ^bundance #63546:2-Pentanol, 4-methyl- 46

6.40 6.60 6.80 7.00 5000 “raTz 43.00 9.65%

27

Tife-> i?,%,-,|J„|l...|...,|,lll T .,, 111.. I,.,. I,,, 11,,.. I,... 1, 1. 11,1.. I.,., I,.,, I,.,, I.... 11 10 15 20253035404550556065 70 75 80859095 100105 Abundance #62568:2-Butanol 45 6.40 6.60 6.80 7.00 m/z 44.05 8.08% 5000

31 59

Tife-> .... ,.4^1. ""i""|i*.l|.. ........................................ TTyTTTrpTTTpTTTpTTTpTTTJTTTTJTTT^^ 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 6.40 6,60 6.80 7.00

24334.D NP103001.M Wed Nov 07 10:39:22 2001 Page 4

NYC-WTC_000068251

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NYC-WTC_000068251Source: NYC Law Department, mirrored locally

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