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GCMS analysis results for sample AD24334, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of environmental sample AD24334 with detection of unknown compounds.

NYC-WTC_000068240–000068254

Folder label: “508 GCMS Scan X 10/11/01 An 11/2/01

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Scanned page image, NYC-WTC_000068250
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data Pile : C:\HPCHEM\1\DATA\NOV0101\24334.D vial: 10 Acq On : 1 Nov 2001 11:48 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.57 0.46 ug/1 75345 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hexaiiol 102 C6H14O 000623-37-0 74 2 2-Propanol, 2-methyl- 74 C4H1O0 000075-65-0 33 3 2,3- tanediol, 2,3-dimethyl- 118 C6H14O2 000076-09-5 33 4 Prop e, 2-ethoxy-2-methyl-_____ 102 C6H14O 000637-92-3 33 (Abundance/ Scan 166 (6.566 min): 24334.D {-) m/z 59.05 100.00%

5000 73

43 51 6.40 6.60 6.80 7.00' 86 100 ........ n+TTT lllll..... .. Tj I II 1.11 11.11111... |. I m/z 54.95 ■nfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 I ^biBidance #63528:3-HexanoI

73 5000 31 6.20 6.40 6.60 6.80 7.00 m/^ 73.00 49.23% '“ . i> I 1 11 >1 -rrrpTT-r|-tTTt^TTTTp-rTT +lllfTTTrpTTTJTt4lpTTTJTTTTpTTrjTTTTJTTTTpT^^

Tlfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 Abundance #62574:2-PropanoI, 2-niethyl-

...... 6.^ 6.^ 6W 6.80 7.00 253 in/z 43.00 24.86% 31 41 i,l|ilii^^ii| ri.|i.l,| lli|ii.i| p-rTTpTTTpTTTTpTT-rjTTrrpT-^ nZz-> 20 25 30 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 Abundance #64429:2,3-Butanedtol, 2,3<jimethy»- 6.^' 's.^' iro' 'e.^' '7.06 “iriTz 41.05 17?^

5000 43 67 T 103 I , , ,, I 1 I , I I , , , , I , ,. , I ,, I, I ,, , , I . ,. . ,, .. , I ,, I , I , H I 1 , I Tlfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 6.20 6.40 6.60 6.80 7.00

24334.D NP103001.M Wed Nov 07 10:39:20 2001 Page 3

NYC-WTC_000068250

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NYC-WTC_000068250Source: NYC Law Department, mirrored locally

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