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GCMS analysis results for sample AD24288, Nov 5 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24288 conducted on November 5, 2001, noting unknown compounds.

NYC-WTC_000068131–000068144

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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Scanned page image, NYC-WTC_000068140
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NYC 9/11 Public Portal Document

Library Search Compound Report Data Pile : C:\HPCHEM\1\DATA\OCT3101\24287.D Vial: 8 Acq On : 31 Oct 2001 10:57 pm Operator: 209 GALOS Sarr^jle : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Paramss LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanol Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.67 0.45 ug/1 61720 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hex^ol 102 C6H14O 000626-93-7 83 2 2-Pei^anol, 4-methyl- 102 C6H14O 000108-11-2 74 3 2-Bi^anol 74 C4H10O 000078-92-2 50 4 2-]^ntanol, 3-methyl- 102 C6H14O 000565-60-6 40 ^bundancad Scan 177 (6.668 min): 24287.D (-) m/z 44795 100.00% 4b

5000

69 I . . , f . l~l . , 41 6.40 6.60 's.so 7.00 , 49 53 ^59 8487 m/z 69700I 19.16% TiZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63584:2-Hexanol *1)5

5000 6.40 6.60 6.80 7.00 69 m/z 41.05 12.93% 19 2731 4^1 56 I 8487 11 II 111111111111111111111111 II 11 n I tm-rrr.. 111 iTp-n-i । i i , 11. ii i | i i . 11111 11 . I 11| . . . i । ■ Tlfe-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Mxindance #63546:2-Pentanol. 4-methyl- 4)5

6.40 6.60 6.80 '7.60

t 5000 m/z 43.05 10.37%

27 19 I 31 42 57 ? 8487 r ‘ ‘' I'''' 1'''' I'' ‘' 1' ‘‘ I tTT-,f,T,,|ll.TTr.-| ‘ I ‘ ‘ ‘' I ‘ ‘ ‘' I' ‘' I'" 11' I" I ‘ ‘ nfe-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #62568:2-Butanol 4)5 6.40I 6.60 6.80 7.00 m/z 44.00 9.93% 5000

27 59 ... .... 72............. " I ‘' I ‘‘ ‘ I “ " I" ‘ ‘ I ‘ ‘‘ 1 ‘ ‘ ‘ ‘ I' ‘ ‘ ‘ * 1 ‘ ‘ 1 ‘ ' 1 ‘ ' I ' • ‘ ’ Tife-> 10 15 20253035404550556065 70 75 80^ 90 95 6.40 6.60 6.80 7.00

24287.D NP103001.M Fri Nov 02 11:59:50 2001 Page 2

NYC-WTC_000068140 '

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NYC-WTC_000068140Source: NYC Law Department, mirrored locally

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