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GCMS analysis results for sample AD24288, Nov 5 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24288 conducted on November 5, 2001, noting unknown compounds.

NYC-WTC_000068131–000068144

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\OCT3101\24287.D Vial: 8 Acq On : 31 Oct 2001 10:57 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T, EstConc Area Relative to ISTD R.T. 7.70 1.21/hg/l 165138 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pent .one, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 50 2 Aceti/ acid, 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 33 3 MoroXoli^^e, 4-methyl- 101 C5H11NO 000109-02-4 9 4 Ac^one 58 C3H6O 000067-64-1 9 Abundance Scan 289 (7.696 min); 24287.D (-) m/z 42.95 100.00% 40

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101 83 7.40 7.60 7.80 8.00 .......... 39 „ +-r 71 • I • I • > ■ I I I • ' I 1 I m/z 59.05 47.05% infe-> 10 20 30 40 50 60 70 80 90 100 110 ^bundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 40

5000 59 ' 7.^' 7.60 'yio' 's.oo' m/z 101.05 21.68%

nA!-> ' 'lb' ‘ 27 I I ’ '30' -r+ « .T • I • ' • ■ I •'■ ■ ■ I • • ■ I ) • ■ • • I • 40 50 60 70 80 90 100 110 Abundance #3292: Acetic acid, 1,1 -dimethylethyl ester 40 ., ,, . I . , ■,

7.40 7.60 7.80 8.00 50)0 57 m/z 58.05 15.93% 101 15 27 1 ■ I • • •'> I ■ ■ ■ ■ I I t-n-r ' I ‘ ' I Tnlz.-> 10 20 30 40 50 60 70 80 90 100 110 4burxlance #63448: Morpholine, 4-methyl- ........ ............ 4)3 7.40 7.60 7.80 8.00 m/z 41.05 6.40% 5000

101 56 71 82 87 93 || VWvvVtvvvz ’ I ‘ ' I ' ‘ ' I ' r-H ■n&-> 10 20 30 40 50 60 70 '' 'go*'' 100 '' i-io 7.40 7.60 7.80 8.00

24287.D NP103001.M Fri Nov 02 11:59:52 2001 Page 3

NYC-WTC_000068141

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NYC-WTC_000068141Source: NYC Law Department, mirrored locally

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