Laboratory report documenting GCMS analysis of sample AD25604 conducted on November 28, 2001, noting unknown compounds.
NYC-WTC_000069803–000069813Folder label: “GCMS Scan X 10/27/01 An 11/17/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C;\HPCHEM\1\DATA\NOV1601\25604.D Vial: 13 Acq On : 17 Nov 2001 2:44 am Operator: 209 GALOS Sample : gc/ms luiknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 2.49 ug/1 447186 1,4-Dichlorobenzene-d4 11.71
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Pentanone; 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 42 2 Acetone 58 C3H6O 000067-64-1 9 3 MorphoZine, 4-methyl- 101 C5H11NO 000109-02-4 9 4 Acetj^ acid, 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 9 Abundance Scan 288 (7.688 min): 25604.D (-) m/z 42795 100.00% 413
59 5000
101 T 7.40 7.60 7.80 8.00 + 71 83 m/z ' I ' ' ' ' I ‘ I ' 1 I ‘ ' I 59.05 51.74% itiZz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 413
5000 -.. 11—. I.. I b I I . . . 59 7.40 7.60 7.80 8.00 m/z 101.05 23.01% 27 101 I I 83 nfe-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62322: Acetone 4|3
7.40 7.60 7.80 8.00 5000 m/z 58.05 19.96% 58 27 • ■ ' I ' ' I ' ' ' ' I ' ' ‘ ‘ I ' ' ' ‘ I ' ' ' ' 1 ' ' ' ' I nZz-> 10 20 30 40 50 60 70 80 90 100 110 ■Abundance #1640: Morpholine, 4-methyk <113 7.^ 7,^ 7.^ 8.00 m/z 41.05 6.50%
5000
15 101 27 71 -X-tn I 56 I 1 ' ' ‘ ' 1 ' I I I 1 1 1 I I I ' ' ' ' I ' ' I ‘ ' I ■ ' • ■ I ' ' ' ' I Tlfe~> 10 20 30 40 50 60 70 80 90 100 110 7.W 7.OT" 7.^ 8.00
25604.D NP103001.M Tue Nov 27 09:43:31 2001 Page 2
NYC-WTC_000069812
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NYC-WTC_000069767
Gas chromatography-mass spectrometry analytical results for sample AD25601 analyzed on November 28, 2001, identifying other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000070032
DEP laboratory report documenting GC/MS results for sample KD25735 analyzed on November 29, 2001.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000070054
DEP laboratory report documenting GC/MS results for sample AD25737 analyzed on November 29, 2001.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068485
Laboratory report documenting GCMS analysis of sample AD24476 conducted on November 14, 2001, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069999
Laboratory report documenting GCMS analysis of sample AD25732 conducted on November 29, 2001, noting other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069676
Laboratory report documenting GCMS analysis of sample AD25462 conducted on November 26, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069896
Laboratory report documenting GCMS analysis of sample AD25735 conducted on November 29, 2001, noting other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069885
Laboratory report documenting GCMS analysis of sample AD25734 conducted on November 29, 2001, noting other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069095
Laboratory report documenting GCMS analysis of sample AD24947 conducted on November 19, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000070143
DEP laboratory report documenting GC/MS results for sample AD25841 analyzed on December 6, 2001.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000070010
Laboratory report documenting GCMS analysis of sample AD25733 conducted on November 29, 2001, noting other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069040
Laboratory report documenting GCMS analysis of sample AD24880 conducted on November 19, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000069728
Department of Environmental Protection GCMS scan log entry dated October 27, 2001.
Filed in the same folder
NYC-WTC_000069729
Log sheet recording liquid-liquid extraction parameters and sample processing details for October and November 2001.
Filed in the same folder
NYC-WTC_000069732
Calibration table listing standard compounds and response values for GCMS analysis dated November 16, 2001.
Filed in the same folder
NYC-WTC_000069742
Laboratory report documenting GCMS analysis of sample AD25599 conducted on November 28, 2001, noting unknown compounds.
Filed in the same folder
NYC-WTC_000069754
Laboratory report documenting GCMS analysis of sample AD25600 conducted on November 28, 2001, noting unknown compounds.
Filed in the same folder