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GCMS analysis results for sample AD24288, Nov 5 2001

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Laboratory report documenting GCMS analysis of sample AD24288 conducted on November 5, 2001, noting unknown compounds.

NYC-WTC_000068131–000068144

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3101\24287.D Vial: 8 Acq On : 31 Oct 2001 10:57 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Benzene-1,2,3,4-d4-, 5,6-dichi Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.52 ug/1 71089 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 T^tative ID MW MolForm CAS# Qual 1 Benzene-1^,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 53 2 1,4-DichI^robenzene-d4 150 C6C12D4 003855-82-1 50 3 Benzald^yde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 35 4 2-Methyl-6-nitroaniline____________ 152 C7H8N2O2 000570-24-1 25 Abundance Scan 711 (11.570 tnin): 24287.D (-) Tm/z 149.90 100.00% Ito

5000 115

52 78 40 1120 11.40 11.60 11.80 12.to T^Jn- m/z 151.90 65.07% Tlfe-> to 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1.2,3,4-d4-, 5.6<lichloro- l$o

115 5000 52 78 11^ 11.40 11,60 11.80 12.00 m/z 114.90 44.56% 87

nZz-> ' to 35 I 40"' to to I ' I' ‘‘ I' 70 80 90 100 110 120 A I'''' I 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4

115 liiO £ 1120 11.40 11.60 11.80 12.00 m/z 52.00 20.06% 5000 52 78

Abundance 30 35 40 50 uu 60 70 80 90 100 110 120 130 140 #66892: Benzaldehyde. 2-hydroxy-3-methoxy- 150 160 T Ite 1120 11.40 11.60 11.80 12.00 m/z 77795 19777% 106 5000 53 81

.T.. Ito...... 1 • ’ u ' ‘ ‘ I ‘ * I • • ' « I nZz-> to 40 to to 70 to 90 100 110 120 130 140 150 160 11.20 11.40 Itto ulto 12.00

24287.D NP103001.M Pri Nov 02 11:59:55 2001 Page 4

NYC-WTC_000068142

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NYC-WTC_000068142Source: NYC Law Department, mirrored locally

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