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GC/MS calibration table for TCLP analysis, Oct 18 2001

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Calibration data table for TCLP analysis using GC/MS standards processed on October 18, 2001.

NYC-WTC_000088491–000088503

Folder label: “GC/MS Scan 9/26/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\OCT1801\LB.D vial: 2 Acq On : 18 Oct 2001 5:09 pm Operator: 209 GALOS Sample : lab blk 10/15 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 6.62 0.47 ug/l 45594 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanp<L 102 C6H14O 000623-37-0 74 2 3-Pent^ol 88 C5H12O 000584-02-1 42 3 2,3-:^tanediol, 2,3-dimethyl- 118 C6H14O2 000076-09-5 42 4 3-P^tanol, 2-methyl- 102 C6H14O 000565-67-3 38 Abundance/ Scan 172 (6.616 min): LB.D (-) m/z 59.05 100.00% J 5b

73 5000 43 ^-,/>, |Z| -o I i-r- 6.20 6.40 6.60 6.80 7.00 84 100 " 1"" I'"' I"" 1' "hl "" I"" 4+ TTprrlyrrTTpnT-rpTTT^^ mT^ 55.00 82.52% ■nZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63530: 3-Hexanol . 5^

73 5000 6.20 a40 a60 a8g 7tg 31 m/z 73.00 50.10% 45 84 +4 I' " ' I " " I' ' " I Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #62943:3-Pentanol 5b I . I

31 6.20 a4p a60 6,80 7t0 5000 m/z 42.95 28.95% 41

'"l'n'-|lll.|....|,.nt,ll I " " I' " ' I' " ' I " '' I AJ -rq-m-rp- Tife-> 20 25 30 35 40 45 50 55 60 65 70 .75 80 85 90 95 100 105 110 Abundance #64428: 2,3-Butanediol, 2,3-dimethyl- 5b 6^0 6.40 6.60 6.80 7.00 m/z 41.00 28.11%

mil 43 85 67 103 rI r I n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.20 6.40 6.60 6.80 7.00

LB.D NP091101.M Fri Oct 19 10:25:51 2001 Page 3

NYC-WTC_000088499

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NYC-WTC_000088499Source: NYC Law Department, mirrored locally

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