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GC/MS calibration table for TCLP analysis, Oct 18 2001

Machine-extracted title · confidence 100%

Calibration data table for TCLP analysis using GC/MS standards processed on October 18, 2001.

NYC-WTC_000088491–000088503

Folder label: “GC/MS Scan 9/26/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1801\LB.D Vial: 2 Acq On : 18 Oct 2001 5:09 pm Operator: 209 GALOS Sample : lab blk 10/15 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hexanol, (R)- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

6.73 0.59 ug/1 57269 1,4-Dichlorobenzene-d4 11.77

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexan61, (R)- 102 C6H14O 026549-24-6 83 2 2-Hex^ol 102 C6H14O 000626-93-7 74 3 2-Peiiranol, 4-methyl- 102 C6H14O 000108-11-2 74 4 2-1 xanol, (S) - 102 C6H14O 052019-78-0 43 ^bundanc< Scan 184 (6.726 min): LB.D (-) m/^ 44.95 100.00%

.L. 40

25a —m-PT-Fn I , , , , I , , .... , —, I , , I 41 6.40 6.60 6.80 7.00 84 87 ......................... I m/z 41.00 16704% 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 ^Kbundance #1794: 2-Hexanol, (R)- 40

5000 6.40 6.60 6.80 7.00 m/ z 69.10 15.22% 69 I " ' • I " '«I " ’' I " «' I ’ " ' I' " ' I " " I " ' ‘ I' ‘' I " nZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63582:2-Hexanol 40 A

6.40 6.60 Is 6.80 7.00 5000 m/z 43.05 12.17%

27 69 19 31 4: 57 I 8487 I'''' I'''' I'''' I' .................. I' H 1 " 111111" " I'' " I' ’' 11 ’' " I " " I " n/z-> Abundance 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 #1773: 2-Pentanol, 4-methyl- 4|5 jy 6.40 6.60 6.80 7.00 m/z 44.00 10.59%

5000 I 69 27 4; 57 I 84 87 I"' ‘ I" " I''" I' 71 T .......................................................... .........................."I" ■n/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00

LB.D NP091101.M Fri Oct 19 10:25:52 2001 Page 4

NYC-WTC_000088500

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NYC-WTC_000088500Source: NYC Law Department, mirrored locally

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