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GC/MS calibration table for TCLP analysis, Oct 18 2001

Machine-extracted title · confidence 100%

Calibration data table for TCLP analysis using GC/MS standards processed on October 18, 2001.

NYC-WTC_000088491–000088503

Folder label: “GC/MS Scan 9/26/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1801\LB.D Vial: 2 Acq On : 18 Oct 2001 5:09 pm Operator: 209 GALOS Sample : lab blk 10/15 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS7’5K.L ★******************************************************************** Peak Number 5 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.75 1.14 ug/1 110640 1,4-Dichlorobenzene-d4 11.77 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pent^one, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 74 2 Hydr^ine, 1,1-bis (1-methylethyl)- 116 C6H16N2 000921-14-2 23 3 CH2ZCHCH2C(O)OCH3 100 C5H8O2 003724-55-8 10 4 Acetone 58 C3H6O 000067-64-1 9 Abundance Scan 295 (7.745 min): LB.D (-) m/z 42.95 100.00% 43

59 5000

101 T^lll|ll‘i|fTTTTy 7.40 7.60 7.80 8.00 8.3 ,1 I" " I " ' 11" " I pTTTp-rrrpTTTp-rrrpTTTpTTrpT^^ 207 m/z 59.05 51.24% Ti/z-> :20 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 Abundance! #64274; 2-Pentanone, 4-hydroxy-4-methyl- 43

5000

27 59 . I.u. _Y40__7;60_Z8g_8t0___ m/z 100.95 18.74% I I

Ln pTr. .,-q- T TiZz-> :20 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 Abundance! #3324: Hydrazine, 1,1-bis(1-methylethyl)- 5|9

I" 7.40 7.60 7.80 8.00 5000 m/F” 58.05 17.09% 101 42 116

. h. li,,p,U|i 7,3 84 I" " I"'' r'" I' ’" 1" ‘' I 1""I""I nfe-> 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 Abundance #1448: CH2=CHCH2C(O)OCH3 43 7.40 7.60 7.80 8.00 m/z 41.00 7.33%

5000

58 I 72 pTT^pTTTykrTTyTTTTJTTT^ 100 p-n-rp-n-rp I 1 I .... I , I . n/z--> 20 30 40 50 60 70 80 90 1001101^30 140 150 160 170 180 190 200 210 7.40 7.60 7.80 8.00

LB.D NP091101.M Fri Oct 19 10:25:54 2001 Page 5

NYC-WTC_000088501

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NYC-WTC_000088501Source: NYC Law Department, mirrored locally

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