GCMS calibration table data, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV1401\LB.D Vial: 10 Acq On : 15 Nov 2001 1:23 am Operator: 209 GALOS Sample : 10/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 1.36 ug/1 221719 1,4-Dichlorobenzene-d4 11.71

Hit# Of 5 Tentzative ID MW MolForm CAS# Qual

1 2-Pentanoney/4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 56 2 3-Hydroxy-^pentanone 102 C5H10O2 003142-66-3 9 3 5 - Hexen - 2/^one 98 C6H10O 000109-49-9 9 4 Morpholyine, 4-methyl- 101 C5H11NO 000109-02-4 9 Abundance Scan 288 (7.688 min): LB.D (-) m/z 42.95 100.00% 43

5000 59

101 7.40 7.60 7.80 8.00 7183 .......................................................... 207 m/z .............. Tp-mp 59.05 48.75% li/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 40

5000 59 7.40 7.60 7.80 8.00 m/z 101.05 20.72% 27 I I ■nfe-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #1691:3-Hydroxy-2-pentanone 31 53 --- 1—,—,—I—,_ I_ I_ _ _ p-Z,_ , I I O|_ I_ I_ I_ r*

7.40 7.60 7.80 8.00 5000 m/z 58.05 17.25% 45 15 I I"‘'I'"'!'"'I 73 84 102 yrTTT^^rrr^rrrr^rrrryrrrry Tl/Z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #63205: 5-Hexen-2-one 43 7.40 7.60 7.80 8.00 m/z 41.05 8.24% 5000

Tl/z-> xx II 55 I 83 0® ' i"'' I ■'''' I' I " I"'' I" I. ‘' 11" " I " " I' " ' I' " ' I'' " I " ' ‘ I ‘ 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 ' I " ' ‘I " " I' " ' I ‘ ' I' " 7.40 7.60 7.80 8.00

LB.D NP103001.M Wed Nov 21 12:57:46 2001 Page 2

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