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GCMS analysis results for sample AD24333, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24333 with detection of unknown compounds on November 27, 2001.

NYC-WTC_000068737–000068747

Folder label: “GCMS Scan X 10/15/01 A 11/3/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\NOV0101\24333.D Vial: 9 Acq On 1 Nov 2001 10:50 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.70 0.74 ug/1 106942 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanon^ 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 39 2 3-Hydroxy/2-pentanone 102 C5H10O2 003142-66-3 23 3 5-Hexen/^-one 98 C6H10O 000109-49-9 10 4 Morphyline, 4-methyl-_____________ 101 C5H11N0 000109-02-4 9 Abundance ' Scan 289 (7.700 min): 24333.D (-) m/z 4^795 100.00% 4(3

59 5000

101 7.40 .J 7.60 7.80 8.00 ....................... I ' ' ‘ ' I ' ' ' ' I ' I ' ' ' I I ' ' ' ' I ■ m/z 59.05 53.53% Tlfe-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #3245; 2-Pentanone, 4-hydroxy-4-mefhyl- 4(3

lililil 59 7.40 7.60 7.80 8.00 m/z 100.95 22.24% 31 101 I I ■ I l'' ■ ' I ' '‘'■I'l 73 ' I ' ' ' n ' ‘ ' I ' TiZz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1691; 3-Hydroxy-2-pentanone 3|1 59 .. 1.,.. I. I .... 7.40 _A60_7;8p__8W^_ 5000 m/z 58.05 18.08% 45 15 I l\ I , 66 73 84 I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' 102 nfe-> 10 20 30 40 50 60 70 80 90 100 110 Abundance

u #63205; 5-Hexen-2-one 4(3 7.40 7.60 7.80 8.00 rn/z 41.05 8.70%

ass 55 38, 50 , I rq—rh-H- 98 ' I ' ' ' ‘ I ' ' ' ' I ''' ' I ' ' I ' ' ' ' I ' Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00

24333.D NP103001.M Tue Nov 27 08:07:51 2001 Page 1

NYC-WTC_000068745

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NYC-WTC_000068745Source: NYC Law Department, mirrored locally

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