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GC/MS analysis results for sample AD25049, Nov 28 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD25049 conducted on November 28, 2001.

NYC-WTC_000069357–000069368

Folder label: “GCMS Scan X 10/23/01 An 11/9/01

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Scanned page image, NYC-WTC_000069365
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV0 901\25049.D Vial: 5 Acq On 9 Nov 2001 4:20 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.68 2.36 ug/1 381123 1,4-Dichlorobenzene-d4 11.72

Hit# of 5 Tent^ive ID MW MolForm CAS# Qual

1 2-Pentanon^< 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 47 2 5-Hexen-2^ne 98 C6H10O 000109-49-9 9 3 3-HydM^-2-pentanone 102 C5H10O2 003142-66-3 9 4 Morpholine, 4-methyl- 101 C5H11N0 000109-02-4 9 Abundance Scan 288 (7.685 min): 25049.D (-) m/z 4^790 100.00% 4(3

59 5000

101 7.40 7.60 7.80 8.00 3? I I ' ' ' ' I ' ' ' ' I ' ' ' ‘ I ' 51 , 69 ¥ ' ' I ' ' ' ' I ' ■ ' I I I ■ ■ ■ I in/z 59.05 50.79% 10 20 30 40 50 60 70 80 90 100 110 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 4(3

5000 59 7.40 7.60 7.80 8.00 m/z 100.95 22.24% 27 8,3 . .... .. . vlz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63205: 5-Hexen-2-one 4(3

7.40 7.60 7.80 8.00 5000 m/z 58.05 16.84% 55 38 , 50 I ' ' I ' ' ‘ ' I ' ' ' ' I 83 ' I ' ' ' ' I ‘ 98 ■ I I I ' ’ ■ I niz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1691:3-Hydroxy-2-pentanone T 31 7.40 7.60 7.80 8.00 m/z 40.95 7.84%

5000 45 15 I I ' ' ' ' I ' ' ' ' 1 ' ' ' ' I rn—r—r-Y-rh-n-n—T-n—p-r— ■nfe-> 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00

25049.D NP103001.M Tue Nov 27 11:09:11 2001 Page 1

NYC-WTC_000069365

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NYC-WTC_000069365Source: NYC Law Department, mirrored locally

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