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← Document results/DEP Box 60/GCMS Scan X 10/2/01 An 10/17/01
Document / 11 pages

GCMS calibration table, Oct 17 2001

Machine-extracted title · confidence 90%

Laboratory report detailing GCMS analysis of sample AD22558 conducted on October 1, 2001.

NYC-WTC_000067428–000067438

Folder label: “GCMS Scan X 10/2/01 An 10/17/01”

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Scanned page image, NYC-WTC_000067436
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1701\LB.D vial: 2 Acq On : 17 Oct 2001 2:09 pm Operator: 209 GALOS Sample : lab blk 10/2 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.76 0.78 ug/1 83030 l,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolPorm CAS# Qual 1 2-Pentanone, 4/hydroxy-4-methyl- 116 C6H1202 000123-42-2 50 2 Acetone 58 C3H6O 000067-64-1 9 3 Morpholine 4-methyl- 101 C5H11N0 000109-02-4 9 4 Acetic aqil , 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 9 Abundance Scan 296 (7.756 min): LB.D (-) ra/z 42.95 100.00% 4(3

59 5000

101 ‘ I ‘ ‘ ‘ I ‘ 7.40 7.60 7.80 8.00 83 m/^ 59.05 51.68% nZz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64275:2-Pentanone. 4-hydroxy-4-methyl- 43

5000 59 7.40 7.60 7.80 8.00 m/z 100.95 19727% 15 31 I ' I ‘ 83

L-t I ■ ‘ ‘ ‘ I • ' “ I ‘ r-p-r-r-rj-r-r-T-r-r-T-r-r-r-p •nfe-> 10 20 30 40 50 60 70 80 90 ioo i-io Abundance #94: Acetone 43

7.40 7.60 7.80 8.00 5000 m/^ 58.05 16.17% 15 58 27 1-r^- ' 1 ' ' ' ' I ' ' ' • I ' ' ' ' I ' ' ' ' 1 ' ‘ ' I ' Tlfe-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1640; Morpholine, 4-tnethyl- 4|3 7.40 760 7.80 8.00 m/^ 41.05 6.87% 5000 101 15 71

■nfe-> 10 20 J,, 30 I 5® • 1 I I ■ ■ I ■ ■ I ' p 40 50 60 70 ■ 1 • • ' ' p ■ ' ■ I ■ • • ■ p 80 90 100 110 7.40 7.60 7.80 8.00

LB.D NP101901.M Tue Oct 23 12:52:53 2001 Page 3 ’ ’NYC-WTC_OOOO67436

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NYC-WTC_000067436Source: NYC Law Department, mirrored locally

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Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.

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