GCMS calibration table data, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C;\HPCHEM\1\DATA\NOV1601\LB.D Vial: 9 Acq On : 16 Nov 2001 10:50 pm Operator: 209 GALOS Sample : lb 10/27 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 1.90 ug/1 317848 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Teiitative ID MW MolForm CAS# Qual 1 2-Pentanon^ 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 72 2 Acetone / 58 C3H60 000067-64-1 9 3 Morpholine, 4-methyl- 101 C5H11N0 000109-02-4 9 4 Acetiq/acid, 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 9 Abundance Scan 288 (7.691 tnin); LB.D (-) m/z 43.00 100.00% 43

59 5000 101 7.^ J, 7,^ 7.^ ‘a.oo ... 207 m/z 59705^ 48.15% T I”"! ■nfe-> 10 20 30 40 50 60 70 80 90 1tX)110120130140150160170180190200210 tessas we #64274:2-Pentanone, 4-hydroxy-4-methyl- 43

—1111111111 Piprn '111111 5000 59 7.40 7.60 7.80 8.00 m/z 100.95 23.81% 27 . 1

-,ju I I -nVp 11'11. J. .Ml I. I.. I ■.. I j I'l«111.11 ( i i.. I 10 20 30 40 50 60 70 80 90 10011012)130140150160170180190200210 Abundance #6; Acetone 43

7.40 7.60 7.80 8.00 5000 m/z 58.05 19.66% 58 27 i-lli'l HI I'l'h 11111 r T I'”*l T i”"i t:Zz-> 10 20 30 40 50 60 70 80 90 1(K)110120130140150160170180190200210 Abundance #1640: Morpholine, 4-methyt- r-r-r-p-j 43 7.40 7.60 7.80 8.00 mTz 41.05 8.52% 5000 101 71

nfe-> XXt 1 56 I 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 7.40 7.60 7.80 8.00

LB.D NP103001.M Tue Nov 27 09:52:04 2001 Page 3

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