Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
NYC-WTC_000087132–000087155Folder label: “508 Scan 9/18/01 9/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0101\LBE.D Vial: 5 Acq On 1 Oct 2001 5:38 pm Operator: 209 GALOS Sample 9/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ******************************* * * ************************************ Peak Number 5 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 7.77 0.81 ug/1 112694 1,4-Dichlorobenzene-d4 11.78 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanprfe, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 53 2 Acetic/dcid, 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 28 3 Morpholine, 4-methyl- 101 C5H11N0 000109-02-4 9 4 3-Hydroxy-2-pentanone 102 C5H10O2 003142-66-3 9 'Kbundang^ Scan 297 (7.770 min): LBE.D (-) m/z 42795 100.00% 40
59 5000
101 ~~ ''I I ' I I I ‘ ' I ' ' 'Vp-Ti-Tj-r 69 83 _740__A6g_r80__8;00__8^ ' I ' ' ' ' I ' ‘ ' I I I ■ I I ■ I ' m/z 59.05 55.55% n/z~> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 40
5000 59 7.40 7.60 7.80 8.00 8.20 23.27% 27 101 ........................... I I ......... 83 10 20 30 40 50 60 70 80 90 100 110 Abundance #3292: Acetic acid, 1,1-dimethylethyl ester 40 I ' ' ' ' I ' 7.40 7W 7.80 8.00 8.20 5000 57 m/T 58.05 16.43% 101 ''i^ 27 -1+ I-' ' I Ti/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1640: Morpholine, 4-methyl- ________ 40 7.40 7,60Z80 8.00 8.20 m/^ 4 0. 5000 101 15 71 I -pT-r-n—j— -ifn 27 I 56 I ' I ' ' ' ' I ' ' ' ' I ' ' ' ' i ' 7.40 7.60' 7.80 ioO' 8.20 ■n/z-> 10 20 30 40 50 60 70 80 90 100 110
LBE.D NP091101.M Wed Oct 03 14:41:06 2001 Page 5
NYC-WTC_000087142
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NYC-WTC_000087980
Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Calibration data table for TCLP analysis including retention times and response factors for various compounds.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23079 conducted on October 10, 2001, identifying unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.
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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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Series of administrative records documenting Section 508 accessibility scans conducted at the World Trade Center site between September 18 and 27, 2001.
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Technical form recording liquid-liquid extraction parameters including drip rates and pH measurements for WTC samples.
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Gas chromatography-mass spectrometry analytical report for sample AD22548 completed on 9/27/01 identifying other unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD22549 conducted on September 27, 2001, identifying unknown compounds.
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