Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
NYC-WTC_000087132–000087155Folder label: “508 Scan 9/18/01 9/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound.Report Data File : C;\HPCHEM\1\DATA\OCT0101\LBE .D vial: 5 Acq On : 1 Oct 2001 5:38 pm Operator: 209 GALOS Sample : 9/18 Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hexanol Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 6.74 0.73 ug/1 101670 1,4-Dichlorobenzene-d4 11.78 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Hex^l 102 C6H14O 000626-93-7 83 2 2-PenZanol, 4-methyl- 102 C6H14O 000108-11-2 78 3 2-Butanol 74 C4H10O 000078-92-2 50 4 2-2flexanol, 3-methyl- 116 C7H16O 002313-65-7 40 Abundance Scan 185 (6.742 min): LBE.D (-) m/z 44.95 100.00% 4^□
5000
41 69 56 6.40 6.60 6.80 7.00 •Si;-... 'I"..III..I"-' m/z 69700 16.85% ■n/z-> Abundance 10 15^0 25 3g^^40 45 50 55 60 65 70 75 #63584:2-Hexanol 80 85^0 95 I 5000 ■ I ■ ■ 7) P I I • I 6.40 6.60 6.80 7.00 m/z 41.05 13.67% 69 I........ I '' I''' 11'''' I'''' I''' I i' I'' I'''' I '' nZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63546: 2-Pentanol, 4-melhyl-
6.40 6.60 6.80 7.00 5000 m/z 43.05 11.64%
27 69 4; 57 i 0' ?5 19 20 ' 25''30''35''40''45 '55 I 60 I H *''' I'''' r ''' I'''' I' I'' I'' ‘' r m/z-> 65 70 75 80 85 90 95
u Abundance #62568: 2-Butanol ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I 4)5 6.40 6.60 6.80 7.00 m/z 44.00 9.82%
5000-
27 59 56 72 TTri+Up- I'''' I'''' I'''' I'' tVz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00
LBE.D NP091101.M Wed Oct 03 14:41:04 2001 Page 4
NYC-WTC_000087141
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NYC-WTC_000087980
Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Calibration data table for TCLP analysis including retention times and response factors for various compounds.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23079 conducted on October 10, 2001, identifying unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.
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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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Series of administrative records documenting Section 508 accessibility scans conducted at the World Trade Center site between September 18 and 27, 2001.
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Technical form recording liquid-liquid extraction parameters including drip rates and pH measurements for WTC samples.
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Gas chromatography-mass spectrometry analytical report for sample AD22548 completed on 9/27/01 identifying other unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD22549 conducted on September 27, 2001, identifying unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD22550 conducted on September 27, 2001, identifying unknown compounds.
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