Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
NYC-WTC_000087132–000087155Folder label: “508 Scan 9/18/01 9/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C;\HPCHEM\1\DATA\OCT0101\LBE.D Vial: 5 Acq On : 1 Oct 2001 5:38 pm Operator: 209 GALOS Sample : 9/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 6.62 0.94 ug/1 130968 1,4-Dichlorobenzene-d4 11.78 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Hexani 102 C6H14O 000623-37-0 90 2 3-Pent lOI 88 C5H12O 000584-02-1 42 3 3-Pe: anol, 2-methyl- 102 C6H14O 000565-67-3 36 4 2-P: ipanol, 2-methyl- 74 C4H10O 000075-65-0 36 ^bundan^ Scan 172 (6.623 min): LBE.D (-) m/z 59.00 100.00% 55
73 5000 43 39 6.20 6.40 6.60 6.80 7.00 49 +4 84 ■ra/z 55.00 8^747% Ti/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #63531:3-Hexanol
55
5000 73 6.20 6.40 6.60 6.80 7.00 43 ■m/z 73700 50.79% 39 I'''' I'''' I TTTT+p4+trTTTp-T 41- ■tpTTTpT-rTp-rrr|-TT tVz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #62943: 3-Pentanol 50
31 6.20 6.40 6.60 6.80 7.00 5000 43.05 27.14% 27 41
i ' 'I ' ' ' ' I ........... m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #1781:3-Pentanol, 2-methyl- 50 6.20 6.40 6.60 6.80 7.00 'm/T 41.05 20.65%
Uajc, 5000 31 73 27 55 45 15 69 T 4 H < nrp , <. J, , ,, p , nfe-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 6.20 6.40 6.60 6.80 7.00
LBE.D NP091101.M Wed Oct 03 14:41:02 2001 Page 3
NYC-WTC_000087140
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NYC-WTC_000087980
Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Calibration data table for TCLP analysis including retention times and response factors for various compounds.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23079 conducted on October 10, 2001, identifying unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.
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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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Series of administrative records documenting Section 508 accessibility scans conducted at the World Trade Center site between September 18 and 27, 2001.
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NYC-WTC_000087008
Technical form recording liquid-liquid extraction parameters including drip rates and pH measurements for WTC samples.
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NYC-WTC_000087013
Gas chromatography-mass spectrometry analytical report for sample AD22548 completed on 9/27/01 identifying other unknown compounds.
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NYC-WTC_000087022
Laboratory report documenting GC/MS analysis of sample AD22549 conducted on September 27, 2001, identifying unknown compounds.
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NYC-WTC_000087044
Laboratory report documenting GC/MS analysis of sample AD22550 conducted on September 27, 2001, identifying unknown compounds.
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