Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
NYC-WTC_000087132–000087155Folder label: “508 Scan 9/18/01 9/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0101\LBE.D Vial: 5 Acq On 1 Oct 2001 5:38 pm Operator: 209 GALOS Sample 9/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.49 1.92 ug/1 268153 1,4-Dichlorobenzene-d4 11.78 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexan^e 100 C6H12O 000591-78-6 91 2 2-Hexa;afone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 83 3 Meth; Isobutyl Ketone 100 C6H12O 000108-10-1 58 4 Oxiri ■ne, 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 50 Abundance Scan 157 (6.485 min): LBE.D (-) m/z 42.95 100.00% 43
58 5000
71 85 100 6.20 6.40 6.60 6.80 3711, ........ 'i , , , I , J, ....... ■ ■ ■ ' I................. I ■ ■ m/z 58.05 58.56% 20 30 40 50 60 70 80 90 100 110 120 130 140 <\bundance #63384: 2-Hexanone 43
5000 58 6.20 6.40 6,60 6,80 29 m/z 56.95 16.32% ,1 ,1. /h .,., .... ... .... . Ti/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #11968: 2-Hexanone, 4-hydroxy-3-propyl- 43
58 6.20 6.40 6.60 6.80 5000 29 m/z 437705 15.09%
•nfe-> Abundance r-r-p-r 20 30 40 43 50 60 71
70 I 80 85
90 #63354; Methyl Isobutyl Ketone 100
100 110 120 130 140 140 J/'JV 6.20 6.40 6.60 6.80 m/z 100.00 10.43%
r 5000 58
85 100 67 rr-T-T-n-p I ..... ...... Tl/Z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 6.20 6.40 6.60 6.80
LBE.D NP091101.M Wed Oct 03 14:40:59 2001 Page 2
NYC-WTC_000087139
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NYC-WTC_000087980
Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Calibration data table for TCLP analysis including retention times and response factors for various compounds.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23079 conducted on October 10, 2001, identifying unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.
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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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Series of administrative records documenting Section 508 accessibility scans conducted at the World Trade Center site between September 18 and 27, 2001.
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Technical form recording liquid-liquid extraction parameters including drip rates and pH measurements for WTC samples.
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Gas chromatography-mass spectrometry analytical report for sample AD22548 completed on 9/27/01 identifying other unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD22549 conducted on September 27, 2001, identifying unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD22550 conducted on September 27, 2001, identifying unknown compounds.
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