GC/MS calibration table, Oct 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0101\LBC.D Vial: 3 Acq On : 1 Oct 2001 3:40 pm Operator: 209 GALOS Sample : 9/15 Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.49 0.85 ug/1 125807 1,4-Dichlorobenzene-d4 11.79 Hit# of 5 / Tentative ID MW MolForm CAS# Qual 1 2-Hexanoj4e 100 C6H120 000591-78-6 90 2 2-Hexandne, 4-hydroxy-5-methyl-3-pr 172 C10H20O2 061141-74-0 83 3 Methyl/isobutyl Ketone 100 C6H12O 000108-10-1 58 4 2-Hex^one, 4-hydroxy-3-propyl-______ 158 C9H18O2 062338-17-4 50 Abundance Y Scan 158 (6.489 min): LBC.D (-) p m/z 42.95 100.00% 43

58 5000

71 85 100 6.20 AJ T-pn 6.40 6.60 T 6.80 T=r

ll,..,^,’,„l,ll..... TTTrn.|rr..|"rr........ |liii|ii m/z 58.05 54.39% Tife-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1556; 2-Hexanone 43

58 ' ''I'' ' ■ I . r7>| ..II 5000 6.20 6.40 6.60 6.80 “mTz 41.00 15.65% 27 Tr,TrT4TTTTrrTTTT4p+ 1 ^1^ r'' ’ I'' ' I ‘‘ U "'' I' *'' I ’' ‘' I'''' I'''' r''' I'''' I *''' r • *' i +7 ttZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #15807:2-Hexanone, 4-hydroxy-5-methyt-3-propyl- 4t3

6.20 6.40 6.60 6.80 5000 m/z sYToy 14711% 58 27 Il""l'‘^‘l''l‘l 7 ^9° pT-rrj+tTTp-rT7p-rTT|TTTTp-rTTp-rTT|TTTTJT^^ ttZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63351: Methyl Isobutyl Ketone ■ 4)3 6.20 6.40 6.60 6.80 m/z 85.05 9.63% 5000 58 27 85 100 n .... .......iy \ , •nZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 a20' 6.40 ' 6.OT '

LBC.D NP091101.M. Tue Oct 02 12:17:03 2001 Page 2

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