GC/MS calibration table, Oct 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT0101\LBC.D Vial: 3 Acq On : 1 Oct 2001 3:40 pm Operator: 209 GALOS Sample : 9/15 Inst : GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 6.39 0.41 ug/1 61034 1,4-Dichlorobenzene-d4 11.79 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hex, one 100 C6H12O 000589-38-8 72 2 3-Pe: anone, 2-methyl- 100 C6H12O 000565-69-5 40 3 Hex, e, 2,4,4-trimethyl- 128 C9H20 016747-30-1 38 4 Bu, .ne, 2,2- dimethyl - 86 C6H14 000075-83-2 28 (kbundan^ Scan 147 (6.388 min): LBC.D (-) m/z 43.00 100.00% 43 57

71 5000 100

6.00 a^64g 6,60 6:^ r '"I p-m-p-m-j- I.. T 57.00 89.25% TiZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 Abundance #63358:3-Hexanone 4{3 57

71 ssa 6.00 6.20 6.40 6.60 6.80 100 70.95 62.16% .............. nfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 Abundance #63398:3-Pentanone, 2-methyl- 517 43 6.00 6.20 6.40 6.60 6.80 5000 m/z 100.05 38.05% 100 71 85 +TTTTTTT rTp l"”! n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 Abundance #65107: Hexane, 2,4,4-trimethyl- 413 5|7 6.00 6.20 6.40 6.60 6.80 71 m/z 4170^ 25.20%

5000-

27 99 I" " I 'I" I" " I" " r I 83 113 ..... I TTTT|-

tt/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 6.00 6.20 6.40 6.60 6.80

LBC.D NP091101.M Tue Oct 02 12:16:58 2001 Page 1

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