Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 4, 2001.
NYC-WTC_000087447–000087457Folder label: “GC/MS Scan 9/19/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0101\LBF.D Vial: 6 Acq On : 1 Oct 2001 6:37 pm Operator: 209 GALOS Sample : 9/19 Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 6.48 0.64 ug/1 86145 1,4-Dichlorobenzene-d4 11.79 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2 -Hexanonj 100 C6H12O 000591-78-6 91 2 2-Hexa: .e, 4-hydroxy-5-methyl-3-pr 172 C10H20O2; 061141-74-0 59 3 Meth- Isobutyl Ketone 100 C6H12O 000108-10-1 58 4 2-Hj :anone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 56 Abundanci Scan 157 (6.484 min): LBF.D (-) m/z 42.95 100.00% 4)3
58 5000
71 85 1(W 6.20 6.40 6.60 6.80
nfe-> ...... .... ^rll.... 7l-rrTyTTTTp-rrr|TTT^^ I’"'I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 m/z 58.00 55.52% Abundance #1556: 2-Hexanone 43
58 ...... /........... 5000 6.20 6.40 6.60 6.80 m/z 41.00 15.83% 27 'T'' ‘ ‘ r ''' I' *' ‘ r' ‘' I'' " r ''' I' I) I r '' ‘ r' *' I'''' r ''' r ''' i ‘ ‘' I'''' r ''' I'' " I' *'' I ■
■nfe-> 20 25 30 35 40,45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #15807:2-Hexanone, 4-hydroxy-5-methyl-3-propyl- 4)3
6.20 6.40 6.60 6.80 5000 “inTz 57.00 14.3 9% 58
Abundance ............... I' I .1 72 'i""r ‘" I'' ' I" ‘' I " " 111" I" "I" " I" " I" " I " " I ’' " i " " I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105
4)3 #63350: Methyl Isobutyl Ketone 6.20 m/z 100.05 ft 6.40 6.60 6.80 9.66%
5000
ftL 58
27 85 100 67 p-rTTp-rTijT-rTTp-rTTjTTTT ' r'" I'" ’ I' n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80
LBF.D NP091101.M Wed Oct 03 14:32:42 2001 Page 2 NYC-WTC_000087454
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NYC-WTC_000088491
Calibration data table for TCLP analysis using GC/MS standards processed on October 18, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067979
Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069732
Calibration table listing standard compounds and response values for GCMS analysis dated November 16, 2001.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067428
Laboratory report detailing GCMS analysis of sample AD22558 conducted on October 1, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068400
Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068559
Calibration data table for GC/MS instrument used in TCLP analysis, generated on November 5, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067623
DEP lab report for GCMS analysis of sample AD23914 conducted on October 25, 2001, noting unknown compounds.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068230
Technical data sheet listing calibration standards and response factors for various polycyclic aromatic hydrocarbons.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069271
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 6, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068815
Calibration data sheet for GC/MS instrument listing standards like naphthalene-d8 used for testing on November 6, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067739
Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 25, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069030
Calibration record for GC/MS instrument using TCLP method, listing standard compounds and response data from November 6, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000087156
Gas chromatography-mass spectrometry scan results recorded on September 19, 2001 for environmental samples.
Filed in the same folder
NYC-WTC_000087157
Laboratory report detailing GC/MS analysis of sample vial 6 conducted on October 1, 2001, including method parameters and peak data.
Filed in the same folder
NYC-WTC_000087160
Laboratory report detailing GC/MS analysis of sample vial 6 conducted on October 1, 2001, including method parameters and peak data.
Filed in the same folder
NYC-WTC_000087163
Laboratory report documenting GC/MS analysis of sample AD22578 conducted on October 10-11, 2001, identifying unknown compounds.
Filed in the same folder
NYC-WTC_000087180
Laboratory report documenting GC/MS analysis of sample AD22579 conducted on October 11, 2001, identifying unknown compounds.
Filed in the same folder