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GC/MS calibration data for TCLP method, Oct 2001

Machine-extracted title · confidence 100%

Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 4, 2001.

NYC-WTC_000087447–000087457

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087455
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0101\LBF,D Vial: 6 Acq On : 1 Oct 2001 6:37 pm Operator: 209 GALOS Sample : 9/19 Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Hexanol Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 6.74 0.45 ug/1 61353 1,4-Dichlorobenzene-d4 11.79 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanolz 102 C6H140 000626-93-7 83 2 2-Pentaifol, 4-methyl- 102 C6H14O 000108-11-2 83 3 2-He^nol, (S)- 116 C7H16O 006033-23-4 39 4 2-Bi/tanol 74 C4H10O 000078-92-2 39 Abundance Scan 185 (6.741 min); LBF.D (-) m/z 44.95 100.00%! 4|5

5000 .............. 69 P I Y t I I I I ' f I 56 87 6.40 6,60 6.80 7.00 TTrl-lT^TTpTTTyTTTTp-rTTJ^^ m/z 69.00 18.07% n/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63584: 2-Hexanol 4)5

. /1 ...................................... 5000 6.40 6.60 6.80 7.00 "m/z 41.05 13.81% 69 IQ 27 ..... ............ ..pill I I" " r " 11" " I''" I"' h' I" I t' •' 1 I I IHII I u I nfe-> 10 15 20 25 30 35.40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63547: 2-Pentanol, 4-methyl- 4)5

6.40 6.60 6.80 7.00 5000 “mTz 4^705 12744%

27 69 57 ..... I....... ?8,||| TTl+kTy I p " p " "p "' p' 'I p I" p "' p "' p "' I" " I 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #3355: 2-Heptanol. (S)- 4)5 6.40 6.60 6.80 7.00 m/z 43.95 9.00% 5000

55 2/ I 70 83 101 I"'' p "' p "' p I" I pTTrf+tTTp-TTTTrTTTt^^ TT-yn—rH-T-yn—r—r-rj—r-i—r-r-|—I—r-r-r-*f— p'" p "' p "' I" " I n/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 6.40 6.60 6.80 7.00

LBF.D NP091101.M Wed Oct 03 14:32:44 2001 Page 3

NYC-WTC_000087455

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NYC-WTC_000087455Source: NYC Law Department, mirrored locally

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