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GC/MS calibration table for TCLP analysis, Oct 2001

Machine-extracted title · confidence 95%

Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.

NYC-WTC_000086788–000086807

Folder label: “508 Scan 9/15/01 9/26/01

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Scanned page image, NYC-WTC_000086796
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT0101\LBC.D vial: 3 Acq On 1 Oct 2001 3:40 pm Operator: 209 GALOS Sample 9/15 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L if*****************************************************************-***

Peak Number 3 2-Hexanol Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 6.74 0.43 ug/1 64121 1,4-Dichlorobenzene-d4 11.79 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexayol 102 C6H14O 000626-93-7 83 2 2-Penyanol, 4-methyl- 102 C6H14O 000108-11-2 74 3 2-He/tanol 116 C7H16O 000543-49-7 56 4 2-H^anol, (R) -_______________________ 102 C6H14O 026549-24-6 43 ^bundanc^ Scan 185 (6.737 mtn); LBC.D (-) m/z 45.00 100.00% 4|5

5000

69 56 87 6.40 6.60 6.80 7.00 Il... I' ' I I I I H I I I I I I I I I I » I n n I • I H J m/z 41.00 16.60% Ti/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63584: 2-Hexanol 45

5000 6.40 6.60 6.80 7.00 69 m/z 69.10 15.27% 87 .... ................. ill TTTTt^ I""I n/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63545: 2-Pentanol, 4-methyl- 40 A ■I 6.40 6^ 6.80 7.00 5000 m/z 44.00 11.18%

69 27 39 , 57 87 rrnTf,.! pTT+p4TTpT7Tp-rrr]-rrrTpT^^ Ti/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 ^bundance #64346: 2-Heptanol 40 6.40 6.60 6.80 7.00 m/z 43.05 10.44%

5000

27 I 39 I 70 83 ^01 pTTTyrTTTpTTTyrXpTTTyrTrX l-TTTJTTTTfl+TTpTTTpnTTtrTT^^ 'T' 'TI T~ n/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 6.40 6.60 6.80 7.00

LBC.D NP091101.M Tue Oct 02 12:17:08 2001 Page 3

NYC-WTC_000086796

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