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GC/MS calibration table, Oct 2001

Machine-extracted title · confidence 50%

Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.

NYC-WTC_000086624–000086643

Folder label: “508 Scan

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Scanned page image, NYC-WTC_000086632
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0101\LBC.D Vial: 3 Acq On 1 Oct 2001 3:40 pm Operator; 2 09 GTkLOS Sample 9/15 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library ; C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Hexanol Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 6.74 0.43 ug/1 64121 1,4-Dichlorobenzene-d4 11.79 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexayol 102 C6H14O 000626-93-7 83 2 2-Pen/anol, 4-methyl- 102 C6H14O 000108-11-2 74 3 2-He/tanol 116 C7H16O 000543-49-7 56 4 2-H^anol, (R)- 102 C6H14O 026549-24-6 43 Abundance/ Scan 185 (6.737 min); LBC.D (-) Wz 45.00 100.00% 4^

5000

69 . . I . . . ,I I . . .I . I , . f, . . . I 56 87 6.40 6.60 6.80 7.00 I" 'I I' I' 'I"" I" " I" " I" " 1 "m/z 41.00 16.60% m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90^100105 Abundance #63584:2-Hexanol 4b

5000 T 6.40 6.60 6.80 7.00 69 m/z 69.10 15.27% 19 27 . 56 1 S/ . .................................... iH tTTT]-rrTr)4iTIJTTTTp-ri4jTTTrpTTTyTTT+jTtTTpTrTTp^ nfe-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63545:2-Pentanol, 4-methyl- 4^ A

6.40 6.60 6.80 7.00 5000 m/z 44.00 11.18%

69 2/ 39 , 57 87 TTyTTT+yrlTTpTrTp-rrTp^ nfe-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 ■T-r-r-r-r^^ Abundance #64346; 2-Heptanol 4^ 6.40 6.60 6.80 7.00 m/z 43.05 10.44%

5000

27

n/z-> pTTTpTrrpTTTjrlTTpTTT^^ . . 7I. /O .101 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 6.40 6.60 6.80 I f 7.00 i-j-

LBC.D NP091101.M Tue Oct 02 12:17:08 2001 Page 3

NYC-WTC_000086632

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NYC-WTC_000086632Source: NYC Law Department, mirrored locally

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