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GC/MS TCLP calibration table analysis, October 2001

Machine-extracted title · confidence 95%

GC/MS analysis report with TCLP calibration table data from October 16, 2001.

NYC-WTC_000089030–000089044

Folder label: “GC/MS Scan 9/28/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1501\LB.D Vial: 3 Acq On : 15 Oct 2001 1:28 pm Operator; 209 GALOS Sample ; lab blk 9/28 Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params; LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table.7/16/01 Library ; C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hexanol Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

6.71 0.57 ug/1 62270 1,4-Dichlorobenzene-d4 11.76

Hit# of 5 •Tentative ID MW MolForm CAS# Qual

1 2-Hexan^ 102 C6H14O 000626-93-7 78 2 2-Pen^nol, 4-methyl- 102 C6H14O . 000108-11-2 64 3 2-He^anol, (S) - 116 C7Hi6O 006033-23-4 50 4 Hexane, 1-methoxy-______________ 116 C7H16O 004747-07-3 45 Abundance Scan 182 (6.714 min): LB.D (-) m/z 44.95 100.00% 4)5

5000

69 .. ■ I -fl (-1 ■J', r,, I,,,I,,, I 6.40 6.60 6.80 7.00 41J1 50 I Y . .............................. 98 m/z 69.00 15.40% Ti/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63584: 2-Hexanol 45

, I,,, ■'iw.U, 5000 6.40 6.60 6.80 7.00 m/z 41.05 14.80% 69 5,6 I .8,7 .... ................... '''' I''" 11'" I" " I'" h " " I" " I"' h'''' I"'' I" " I" " 1"'' I 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63545:2-Pentanol, 4-methyl- 4^

■' ' ' I ' ' ' I ' ' ' ‘ I ' ' ' ' I ' ' ' ' I 6.40 6.60 6.80 7.00 5000 piiTz 4^795 13783%

69 ^27- 39- I __ 57__ 4^ . . . .87________

Ju I' I" II • ” • 111" I ■ ■' -p-rT4-p4TTp-rTTp-rTTpTrrp-rTT^ nZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance - #3355: 2-Heptanol. (S)-------- s6760^6?80jnf60- m/z 43.95 9.38%

5000

55 2/ 39 , ......... L............ 70.......... 83............... 101..... ■ .............. . nZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 . 6.40 6.60 6.80 7.00

LB.D NP091101.M Tue Oct 16-15:20:31 2001 Page. 4

NYC-WTC_000089039

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NYC-WTC_000089039Source: NYC Law Department, mirrored locally

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