GC/MS analysis report with TCLP calibration table data from October 16, 2001.
NYC-WTC_000089030–000089044Folder label: “GC/MS Scan 9/28/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\OCT1501\LB.D Vial: 3 Acq On ; 15 Oct 2001 1:28 pm Operator; 209 GALOS Sample ; lab blk 9/28 Inst : GC/MS 209 Mise Multiplr: l.od MS Integration Params; LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title ; 209 625/TCLP calibration table 7/16/01 Library : C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.73 5.08 ug/1 559282 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2 -Pent anoney^^-hydroxy-4 -methyl - 116 C6H12O2 000123-42-2 50 2 Morpholine^ 4-methyl- 101 C5H11N0 000109-02-4 9 3 3-Hydroxy4^2-pentanone 102 C5H10O2 003142-66-3 9 4 Butane ,/i-ethoxy- 102 C6H14O . 000628-81-9 9 abundance Scan 293 (7.733 min): LB.D (-) m/z42.95 100.00% 4b
59 5000-
101 I ' ' ' ' I ' ' ' ' I 7.40 7.60 7.80 8.00 69 83 + ' I ' ' ' ' I ' ' ' ' I ' I I I ' ' ■ I m/z 59.05 52.82% Ti^-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyl- 4(3
5000 59 7.40 7.60 7.80 8.00 m/z 101.05 19.61% 15 31 101 I l| I , , , I I I I , I I............. I |l| I I I I ' ' I ' ' ' . ........ . TiZz-> 10 20 30. 40 50 60 70 80 90 100 110 Abundance #1640: Morpholine, 4-methyl- 413 ' I ' ' ' ' I 7.40 7.60 7.80 8.00 5000 m/z 58.05 16.50% 101 15 71 27 J ' 26' ' ''30 .---------- 56_ I ' ' I ' ' I ' I-' r-|^i-i-rT-|-rT-r-ryT-r-i-r-fL-i-rT^
Tife-> 10 40 50 60 70 80 90 100 110 Abundance - — #1691:3-Hydroxy-2-pentanone ' ' I ‘ ’ 1 ' ' ' ' I ' ' ' ' I,'.fTT ‘r3ll 7.40. 7.60 7.80-.8.00.:.< m/z 41.05 7.65%
5000 -45-r 15 , , I...... II....... I ' ‘ ' I ' ' ' ' I ' ' ' ' I ' 66 73 84 ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ‘ 102 ' I 71ZZ-> 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00
LB.D NP091101.M Tue Oct 16 15:20:34 2001 Page 5
NYC-WTC_000089040
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NYC-WTC_000088491
Calibration data table for TCLP analysis using GC/MS standards processed on October 18, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088700
Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088184
Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089278
GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086624
Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086788
Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087496
Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067739
Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 25, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068559
Calibration data table for GC/MS instrument used in TCLP analysis, generated on November 5, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067428
Laboratory report detailing GCMS analysis of sample AD22558 conducted on October 1, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068400
Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067979
Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
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NYC-WTC_000089025
Fragmented GC/MS scan page from a laboratory blank sample dated September 28, 2001.
Filed in the same folder
NYC-WTC_000089026
Fragmented GC/MS scan page from a laboratory blank sample dated September 28, 2001.
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NYC-WTC_000089045
Laboratory report documenting GC/MS analysis of sample AD23652 conducted on October 16, 2001.
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NYC-WTC_000089059
Laboratory report documenting GC/MS analysis of sample AD23651 conducted on October 16, 2001.
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NYC-WTC_000089073
Laboratory record for sample AD23653 showing detection of unknown compounds on October 16, 2001.
Filed in the same folder