GC/MS TCLP calibration table analysis, October 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1501\LB.D Vial: 3 Acq On : 15 Oct 2001 1:28 pm Operator: 209 GALOS Sample : lab blk 9/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Oxirane, 2,2-dimethyl-3-propyl Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 10.21 0.48 ug/1 52914 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 Tentative ID MW MolForm CAS# Qual■ ’

1 Oxirane, 2,2ydimethyl-3-propyl- 114 C7H14O 017612-35-0 38 > 2 Oxirane, 2-^tyl-3-methyl-, cis- 114 C7H14O 056052-93-8 32 3 Hexane, 1/propoxy- 144 C9H20O 053685-78-2 16 . 4 Hexane, -methyl- 100 C7H16 000591-76-4 12 • Abundance Scan 563 (10.212 min); LB.D (-) m/z 43.00 100.00% 43

5000 59 85 73 9.80 10.00 10.20 10.40 10.60

TlZz-> ..J 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 120 100 m/z 59.05 34.85% Abundance #3Toy Oxirane, 2,2-dimethyl-3-propyl- 43 5P 85

A.................. 5000 9.80 10.00 10.20 10.40 10.60 m7z 55.00 34.26% l"H|'^"|■^l.. . ... p”... ■rTi:' Vt Tlfe-> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 120 Abundance #3063: Oxirane, 2-butyl-3-methyl-. cis- “43' A 55 9.80 10.00 10.20 10.40 10.60 5000 85 m/^ 41.05 33.18% 71 /I

tTTTTTT +TTTrrpT TTtpTTTynTTyrTTTJTTT^^ J I" "I," "I 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 120 Abundance--------- #8516; Hexane, 1-propoxy- ... r.-vr-l— ' ■^<=■413-^^ TsTsoLJo.oo^io.^w.^d^io.edTj 57.00 27.70% 5000

“ 73 85 I 61 Y I'''' I"' M111"" I"" HI" 11"' I'" * I"'' I"" I" 11111111H1111II11111| I! 111111111111111 •nZz-> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 120 9.80 10.00 10.20 10.40 10.60

LB.D NP091101.M Tue Oct 16 15:20:36 2001 Page 6

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