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GC/MS analysis results for sample AD23325, Oct 16 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23325 conducted on October 16, 2001.

NYC-WTC_000088504–000088519

Folder label: “GC/MS Scan 9/26/01

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Scanned page image, NYC-WTC_000088516
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0901\23325.D Vial: 12 Acq On : 10 Oct 2001 12:06 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise ': Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Oxirane, 2,2-dimethyl-3-propyl Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 10.20 0.47 ug/1 50339 1,4-Dichlorobenzene-d4 11.75

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 Oxirane, Z,2-dimethyl-3-propyl- 114 C7H14O 017612-35-0 38 2 Oxirane,/2-methyl-3-propyl-, cis- 100 C6H12O 006124-90-9 38 3 TetrahySrofuran, 2,2-dimethyl- 100 C6H12O 001003-17-4 36 4 Hexanq/ 2-methyl- 100 C7H16 000591-76-4 35 Abundance A Scan 562 (10.203 min): 23325.D (-) m/z 43.05 100.00% 43

5000 57 85 73 9.80 10.00 10.20 10.40 10.60 100 ' I ' ’ ' ' I ' ' ' ' I ’ m/z 56.95 32.70% Tl^-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #3003: Oxirane, 2,2-dimethyl-3-propyl- 43 5P 85

5000 I ' ' ' ' I ' ' ' ' I ' ' 9.80 10.00 10.20 10.40 10.60 72 m/T 55.00 31.67% .^1—S— Tlfe-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #1531: Oxirane, 2-methyl-3-propyl-, cis- 4)3 \ AA A A 9.80 ' 10.00 10.20 10.40 10.60 57 5000 71 85 m/z 59.05 31.43% k

100 ............... I ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' Tl/z-> Abundance 20 30 40 50 60 70 80 #63380: Tetrahydrofuran, 2,2-dimethyl- 90 100 110 120 A 4)3 9.80 10.00 10.20 10.40 10.60 m/ z 41.00 29.16%

5000

.-j-rn I I IT 20 30 40 -.-r-r^UL 50^ 60 59 70 70 80 85

90 100 110 120 9.80 lL 10.00 10.20 10.40 10.60

23325.D NP091101.M Thu Oct 11 12:57:19 2001 Page 5

NYC-WTC_000088516

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NYC-WTC_000088516Source: NYC Law Department, mirrored locally

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