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GCMS Analysis Report for Sample AD26388, Dec 2001

Machine-extracted title · confidence 100%

Report documenting GCMS analysis of sample AD26388 with a note regarding unknown compounds.

NYC-WTC_000031452–000031472

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26388.D Vial: 14 Acq On : 1 Dec 2001 12:02 am Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Oxirane, 2-methyl-3-propyl-, c Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 5.67 0.61 ng/uL 270347 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 entative ID MW MolForm CAS# Qual 1 Oxirane, 2-methyl-3-propyl-, cis- 100 C6H120 006124-90-9 42 2 Oxirane/ 2-methyl-3-propyl-, trans- 100 C6H120 006124-91-0 37 3 Octane, 4-methyl- 128 C9H20 002216-34-4 32 4 2H-Pyran, tetrahydro- 86 C5H10O 000142-68-7 23 Abundance Scan 90 (5.671 min): 26388.D (-) m/z 41.10 100.00% 41

57 85 5000 71 .. S..... A 5.40 5.60 5.80 6.00 - 50 , -4 m/z 43.05 79.79% miz-> 20 30 40 50 60 ’1 70 80 90 100/1110 1120 ‘' 130 Abundance #1531: Oxirane, 2-methyI-3-propyl-, cis- 43

57 5000 71 85 5.401 5.60 5.80 6.00 m/z 44.95 73.38% . n/z—> 20 -l 30 40 -- 1-r 50 60 70 ' 80 100 1 • i • ' 1 1 i ■ ■ ■ ■ I ■ ■ ■ ■ i ■ • ■ ■ i ‘ 90 100 110 120 ‘ ■ i ' ‘ 130 Abundance #1532: Oxirane, 2-methyl-3-propyl-, trans- 41 — • ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ 5.40 5.60 5.80 6.00 _ 5000 57 m/z 57.10 60.10% 71 85

— - 100 ' i » • > * i * * • > । -

MA • • l • • • ‘ I ' ' ' ' l 4 ‘ 1 ‘ I 1IIT yr-r-rT-p-r mz-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #65131: Octane, 4-methyl- 43 5.40 5.60 5.80 6.00 m/z 85.05 48.91%

m/z—> 5000

27 — ----- 20 30 40 50 57

60 71

70 - 80 90 85 ........ -12— 100 110 120 130 Tit 5.40 J W 5.60 5.80 6.00

26388.D NP112701.M Tue Dec 04 10:40:21 2001 Page 4

NYC-WTC_000031461

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