GCMS Analysis Report for Sample AD26388, Dec 2001

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Report documenting GCMS analysis of sample AD26388 with a note regarding unknown compounds.

NYC-WTC_000031452–000031472

Folder label: “GCMS X 11/5/01 A 12/1/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26388.D vial: 14 Acq On : 1 Dec 2001 12:02 am Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C: \DATABASE\NBS75K. L ********************************************************************* Peak Number 5 2-Furanmethanamine, tetrahydro Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.12 2.34 ng/uL 1027330 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Furanmethanamine, tetrahydro- 101 C5H11NO 004795-29-3 40 2 2-Hepten-3-ol, 4,5-dimethyl- 142 C9H180 055956-37-1 40 3 Furan, 2- tyltetrahydro- 128 C8H160 001004-29-1 39 4 Propanoic acid, 2-methyl-, anhydrid 158 C8H14O3 000097-72-3 38 Abundance / Scan 139 (6.120 min): 26388.D (-) m/z 71.05 100.00%

1 71

5000 43 TTTurrfT 57 5.80 6.00 6.20 6.40 TIBB—tu—ur j, nti -f-T 51-1465, I,, 81........... 100............................. 11 1 1 I ‘ 1 ‘ ' 11 ' ’ 1 I ' 1 ' ‘ I ’ ‘ ‘ * 1 ‘ ‘ ‘ 1 1 ‘ m/z 43.05 42.20% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130

La) Abundance #1633: 2-Furanmethanamine, tetrahydro- 71

43 5000 30 OInn———TT 5.80 6.00 6.20 6.40 84 m/z 41.0.5 24.57% 58 1 - Hr ’11 .101............................ miz-> ' 10 120 30 40 50 60 70 80 ' 90 ‘ 100 110 120 130 Abundance #8051: 2-Hepten-3-ol, 4,5-dimethyl- 71 J ■ ■1 i ■ ■ • • i ‘ 1 • 1 । ' i ■ ■ ' * i 5,80 6.00 6.20 6.40 5000 43 m/z 42.10 18.59% 27 15 55 81 ——100 rfu—r109 124 m/z—> Abundance 10 1 I 11 »■ i • • ■»t • ■ • > i •»* • j ‘ • • • । • • • • । • 20 30 40 50 60 —8 TIPBInn 80 #5023: Furan, 2-butyltetrahydro- 90 ' i ■' • ■ i ■ ■ • ■ i ■' 100 110 120 130 * r [ * * > > । > । ■ ■ ■ ■ i 71 5.80 6.00 6.20 6.40 m/z 39.10 10.67%

5000

m/z—> | 42 55 । । I । । i । I 1 1 11 1 1 " 1 I H r 1 1 1 # 1 1 10 20 30 40 50 60 70 80 90 100 110 120 128 130 S . । AMAA 5.80 6.00 6.20 6.40

26388.D NP112701.M Tue Dec 04 10:40:22 2001 Page 5

NYC-WTC_000031462

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NYC-WTC_000031462Source: NYC Law Department, mirrored locally

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