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GCMS Analysis Report for Sample AD26386, Dec 2001

Machine-extracted title · confidence 100%

Report documenting GCMS analysis of sample AD26386 with a note regarding unknown compounds.

NYC-WTC_000031415–000031432

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26386.D Vial: 12 Acq On : 30 Nov 2001 10:13 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Propanoic acid, 2-methyl-, anh Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 6.10 1.08 ng/uL 480759 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative/ID MW MolForm CAS# Qual 1 Propanoic acid, 2- thyl-, anhydrid 158 C8H14O3 000097-72-3 59 2 2-Furanol, tetrahy o-2-methyl- 102 C5H10O2 007326-46-7 43 3 2 - Furanmethanol, tetrahydro- 102 C5H10O2 000097-99-4 40 4 2-Hepten-3-ol, 4, 5-dimethyl- 142 C9H180 055956-37-1 40 Abundance / Scan 138 (6.104 min): 26386. D(-) m/z 71.05 100.00% 71

5000 43

39 55 5.80 6.00 — A 6.20 6.40 m mm.... 4 —Hm 100 I . . j . I > 11 . I . . I . 1 I . I I 1. 11 TI1111 I I I | I I I , I m/z 43.10 43.69% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #11901: Propanoic acid, 2-methyl-, anhydride 71

5000 43 N T12/1/7/1/*1/*/"/111/4/2/1/4TTT 5.80 6.00 6.20 6.40 m/z 41.10 24.06% 4. +38 + 1]Ik..p...551 ... 4!1 .... 1 * m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63475:2-Furanol, tetrahydro-2-methyl- 71 rW T I 5.80 6.00 6.20 6.40 5000 43 m/z 42.05 17.26%

49 55 61 . ,............ 84 TUTOTITT Tm Tpuuan) (11.. 11|, miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63508: 2-Furanmethanol, tetrahydro- • YAr ■ T ;.. • .......... : 71 5.80 6.00 6.20 6.40 43 m/z 39.00 10.49% 5000- 27 M. m/z—> ' ■' i''1 ‘ i' „ll 57 ■ l r- ■ ■ | ■1.. I " " 1 " .11 I।।।।n 11111111 20253035404550556065 70 75 80859095 100 105 - -44 ■ I' 5.80 6.00 6.20 6.40

26386.D NP112701.M Tue Dec 04 10:38:34 2001 Page 4

NYC-WTC_000031426

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NYC-WTC_000031426Source: NYC Law Department, mirrored locally

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