GCMS Analysis Report for Sample AD26386, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26386.D Vial: 12 Acq On : 30 Nov 2001 10:13 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L **************************************************************** * * * * * Peak Number 5 2-Butanol, 3-methyl-, (S)- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.19 10.04 ng/uL 4480040 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Te ative ID MW MolForm CAS# Qual 1 2-Butanol, methyl-, (S)- 88 C5H120 001517-66-4 38 2 2,4-Pentan iol 104 C5H12O2 000625-69-4 33 3 2-Butanol 3-methyl- 88 C5H120 000598-75-4 9 4 Propane, -ethoxy­ 88 C5H12O 000625-54-7 9 Abundance scan 256 (7.186 min): 26386.D (-) m/z 45.00 100.00% 45

5000 61 73

6.80 7.00 7.20 7.40 7.60

m/z—> 35 . .. . Th.... 91....................... TU—ITOUT • •i <> • • l•• •• i 207 Timul|ini| i ui । n n| n ii|iiii] nil jinq 10 2030405060 70 8090 100110 120130140150 160170 180190200210 m/z 43.00 54.69% Abundance #852:2-Butanol, 3-methyl-, (S)- 45

5000- _... 1.......... 1 178 : j i i i i [ iiiijiiitjii 6.80 7.00 7.20 7.40 7.60 m/z 73.05 40.69% 27 1 55 73

mlz—> mH h, ‘ 1 " i ••" I' ‘ 87 111 > 11 11 111 111II i i ii1 > ii11 i I 111ii111ii1 I 111ii1: r 1i 11i11 1111111I It 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #1906:2,4-Pentanediol 45 1 i • ■ ■ ■ i 1 • ■ ■ i 1 1 1 1 I 1 1 1 1 f1 r 6.80 7.00 7.20 7.40 7.60 5000 m/z 61.00 38.29% 71 . 27 15.1.. "i"' IEEII’I’I 89 ,..... 61 Tgmggu |

miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #62962: 2-Butanol, 3-methyl- T [ 188.8 I I I I I 1I I I ] I I I I I I T 45 6.80 7.00 7.20 7.40 7.60 m/z 44.00 10.60% 5000

55 73 ................ 1...... 88........................................................... I . । > ill pt*, fit t: | 1111 {: 111 j i: 1:11 > i > । M 111 11 k 1111111:1111 m : 111. i i j 111 > j Tm-r . । . . . . । f TT । ii i i । । i i i ।r r m/z—> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 6.80 7.00 7.20 7.40 7.60

26386.D NP112701.M Tue Dec 04 10:38:35 2001 Page 5

NYC-WTC_000031427