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GCMS Analysis Report for Sample AD26388, Dec 2001

Machine-extracted title · confidence 100%

Report documenting GCMS analysis of sample AD26388 with a note regarding unknown compounds.

NYC-WTC_000031452–000031472

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26388.D vial: 14 Acq On : 1 Dec 2001 12:02 am Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 2-Butanol, 3-methyl-, (S)- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.19 18.37 ng/uL 8078200 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Butanol, 3-methyl-, (S) - 88 C5H120 001517-66-4 38 2 2,4-Pentanediol 104 C5H12O2 000625-69-4 33 3 2-Butanol, 3-methyl- 88 C5H120 000598-75-4 9 4 Butane, 2-ethoxy-__________________ 102 C6H140 002679-87-0 9 Abundance Scan 256 (7.193 min): 26388.D (-) m/z 45.05 100.00% 45

5000 61 73 ---------- 6.80 7.00 7.20 7.40 7.60 ............... 91 105 207 110111110/1303117 T m/z 43.00 52.47% nfe-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #852:2-Butanol, 3-methyl-, (S)- 45

= P I ! I | -PPTT I ‘ | r l 5000 6.80 7.00 7.20 7.40 7.60 m/z 73.05 42.25% 27 55 73 u. i,I, I I 87 .. I. I.. I .. 111 «...! 111. |. 11111 > >. I’T u |.... j., . > | 11 11111111.... |, H . I ,, , . 11. ., (. 1. 1111 11 111 II 111 11 11111 111 miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #1906: 2,4-Pentanediol 45 1111111*1111111111111 6.80 7.00 7.20 7.40 7.60 5000 m/z 61.10 38.44%

27 71 15 1’1111 I 61 Epug ।.. i. ।।।. 111.. ।.,.. । TT—231—071 89 111" ।।■ 11 ■ •, । miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #62962:2-Butano!, 3-methyl- -rpi i i IT 1-111T ..I..,.!,. 45 6.80 7.00 7.20 7.40 7.60 m/z 44.05 10.62% 5000

27 55 73 tt. ................ 1...... 88..................................................................... TTTmrrrrTrrmi miz—> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 6.80 7.00 7.20 7.40 7.60

26388.D NP112701.M Tue Dec 04 10:40:25 2001 Page 9

NYC-WTC_000031466

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NYC-WTC_000031466Source: NYC Law Department, mirrored locally

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