DEP lab report dated December 4, 2001, documenting GCMS analysis of sample AD26392 noting other unknown compounds.
NYC-WTC_000031530–000031549Folder label: “GCMS X 11/5/01 A 12/1/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26392.D Vial: 5 Acq On : 30 Nov 2001 3:52 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 2-Butanol, 3-methyl-, (S)- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.19 9.21 ng/uL 4028250 1,4-Dichlorobenzene-d4 11.89 Hit# Of 5 'entative ID MW MolForm CAS# Qual l 2-Butanoly 3-methyl-, (S)- 88 C5H120 001517-66-4 38 2 2,4-Pentanediol 104 C5H12O2 000625-69-4 33 3 2-Butanol, 3-methyl- 88 C5H120 000598-75-4 9 4 Acetaldehyde, methoxy- 74 C3H602 010312-83-1 9 Abundance Scan 256 (7.186 min): 26392.D (-) m/z 45.10 100.00% 45
5000 61 73 TO1TTTT 6.80 7.00 7.20 7.40 7.60
miz-> -nll — t+ ml mmmm mmmmpm 11—0011—111 m207. fTTT m/z 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 43.00 54.99% Abundance #852: 2-Butanol, 3-methyl-, (S)- 45
5000 r 1' T T"T it । i । t » ITTT j i t r i | i i 6.80 7.00 7.20 7.40 7.60 m/z 73.05 40.66% 73 ... 2. hu551..... .1.....87 110121111111111171 rrq-mTf irrrrrrrrpT TTTTTTI TUTTUTTTTTTT miz-> 10 20 30 40 50 60 70 80 90100110120130140150160170180190200210 Abundance #1906:2,4-Pentanediol 45 TIIBnn p-r-r5 TTBagTT 6.80 7.00 7.20 7.40 7.60 5000 m/z 61.00 39.22%
27 71
miz-> 15 I I 1415898 4UU 89 TTUIOU TTETIEVLTTTTTT 10 2030405060 70 8090 100110 120 130 140 150 160 170 180 190200210 Abundance #62962:2-Butanol, 3-methyl- —i | । ■ i * । ■ • • ■ । • ■ ■ > | ‘ • I ' ' 45 6.80 7.00 7.20 7.40 7.60 m/z 44.05 10.70%
5000
55 73
m/z—> 27 _________ h. "i” "I ""I LX | 88 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 TTTOTITTIT , rr J ‘1002’0911187 =Tr—mrmmffTTmt 6.80 7.00 7.20 7.40 7.60
26392.D NP112701.M Tue Dec 04 10:43:12 2001 Page 7
NYC-WTC_000031544
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NYC-WTC_000031550
DEP lab report dated December 4, 2001, documenting GCMS analysis of sample AD26393 noting other unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031491
Laboratory comment confirming detection of Butylbenzylphthalate in sample AD26390 on December 10, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031433
Report documenting GCMS analysis of sample AD26387 with a note regarding unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031415
Report documenting GCMS analysis of sample AD26386 with a note regarding unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031473
Report documenting GCMS analysis of sample AD26389 with a note regarding unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031509
Analysis report for sample AD26391 indicating the presence of other unknown compounds on December 4, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031968
Laboratory report documenting GCMS analysis of sample AD26676 identifying unknown compounds on December 10, 2001.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031847
Mass spectrometry analysis of sample AD26537 found no non-target compounds present, Dec 16, 2001.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031384
Report documenting GCMS analysis of sample AD26336 with a note regarding unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032245
Gas chromatography-mass spectrometry analysis of sample AD26832 documenting unknown compounds with reference to comments.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031739
Analysis report dated December 16, 2001, stating that mass spectrometry of sample AD26478 revealed no non-target compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032142
Calibration data sheet listing standard compounds and response factors used for GCMS analysis on December 5, 2001.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000031347
Single-page GCMS document identifier from the Environmental Protection Department archive covering late 2001 testing records.
Filed in the same folder
Document header for GCMS analysis records from the NYC WTC environmental monitoring program.
Filed in the same folder
NYC-WTC_000031350
Calibration data table for gas chromatography-mass spectrometry analysis dated December 3, 2001.
Filed in the same folder
NYC-WTC_000031359
Laboratory comment confirming no non-target compounds were detected in sample AD26203 on December 10, 2001.
Filed in the same folder
NYC-WTC_000031372
Analysis report for sample AD26335 indicating the presence of other unknown compounds on December 4, 2001.
Filed in the same folder