GCMS analysis report for sample AD26392, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26392.D Vial: 5 Acq On : 30 Nov 2001 3:52 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Oxirane, 2-methyl-2-(1-methyle Concentration Rank II R.T. EstConc Area Relative to ISTD R.T.

6.57 0.41 ng/uL 179659 1,4-Dichlorobenzene-d4 11.89

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Oxira , 2-methyl-2-(I-methylethyl) 100 C6H120 072221-03-5 64 2 2-He: none 100 C6H120 000591-78-6 59 3 2-H anone 100 C6H120 000591-78-6 53 4 2-Hexanone Abundance 100 C6H120 000591-78-6 53 Scan 189 (6.572 min): 26392.D (-) m/z 43.00 100.00% 43 58 5000 J * i ’ * ' * i * * 1 * i * 1 * * i * * ' * i * 6.20 6.40 6.60 6.80 7.00

mlz—> 3+4 1. TI—puu71. 85 —umj100 m/z 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 58.10 60.49% Abundance #1530: Oxirane, 2-methyl-2-(1 -methylethyl)- 43 58

5000 CI TT TT T p IIt 6.20 6.40 6.60 6.80 7.00 71 m/z 41.05 15.48%

mz-> m-AP--O——s0, mmm ................. 66 100 11’1 —..... TTTTHTI 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 85

Abundance #63385: 2-Hexanone 43 20 6.40 6.60 6.80 7.00 5000 58 m/z 57.05 11.59% 29

miz-> TpTtr m + 71 --- TOWTTTTTTTOTTT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 85 100

NW Abundance #63384:2-Hexanone 43 6.20 6.40 6.60 6.80 7.00 m/z 100.05 7.46% 5000 58 29

TIT mP TT I 71 85 TTHHmmmm 190 y........ ........ ■nfz~> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80 7.00

26392.D NP112701.M Tue Dec 04 10:43:11 2001 Page 6

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