GCMS analysis report for sample AD26392, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26392.D Vial: 5 Acq On : 30 Nov 2001 3:52 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 ' MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Hep ten-3-ol, 4,5-dimethyl- Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.12 1.51 ng/uL 661263 l,4-Dichlorobenzene-d4 11.89 Hit# Of 5 Tentative ID MW MolForm CAS# Qual l 2-Hepten-3-ol,/4,5-dimethyl- 142 C9H180 055956-37-1 39 2 Propanoic acid, 2-methyl-, anhydrid 158 C8H14O3 000097-72-3 33 3 Cyclopentan 1, 1-methyl- ==* 100 C6H120 001462-03-9 9 4 Cyclopentan 1, 1-methyl - 100 C6H120 001462-03-9 9 Abundance Scan 140 (6.122 min): 26392.D (-) m/z 71.05 100.00% 7 5000 43 TIpnnnnTTTTpuukT T 5.80 6.00 6.20 6.40 - « 57 81 !, 100 • • l • ■ * < l ■ • • ‘ I > 51444 11 • • I ’ ’ * * I'‘*‘I’* ‘ ‘ 120 130 m/z 43.05 41.41%

A m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #8051: 2-Hepten-3-ol, 4,5-dimethyl- 71

5000 43 •r r—--r-r prrttI ri r i I 5.80 6.00 6.20 6.40 27 m/z 41.05 23.03% 15 55 ------ 81 100 ire 124 miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #11901: Propanoic acid, 2-methyl-, anhydride 71 ,*1/1//**1*1/1111/11/1/8"B.R 5.80 6.00 6.20 6.40 43 m/z 42.10 19.20% 5000

27 . m/z-> -374 10 20 30 40 50 55 60 TT I J I II I I I I TTT 70 80 90 100 -*]0PPPPpT 110 TT-p-r-r-q-r 120 130 Abundance #63340: Cyclopentanol, 1-methyl- — ! —TTT . . | 43 71 5.80 6.00 6.20 6.40 m/z 39.10 11.23% 58 5000

85 ................... , 51,1 ■ ■ ।1 ■ ■ ■ । ■ • • ■ । ■ ■'' t • • * ■ । • • • I i * * * * i ।.... J.....100 AAAA miz—> 10 20 30 40 50 60 70 80 90 100 110 120 130 5.80 6.00 6.20 6.40

26392.D NP112701.M Tue Dec 04 10:43:11 2001 Page 5

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