GCMS analysis report for sample AD26392, Dec 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26392 .D vial: 5 Acq On : 30 Nov 2001 3:52 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1-Propene, 3-methoxy­ Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 5.66 0.44 ng/uL 194132 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 entative ID MW MolForm CAS# Qual 1 1-Propene/3-methoxy- 72 C4H8O 000627-40-7 9 2 2-Propen-1-ol, 2-methyl-, acetate 114 C6H10O2 000820-71-3 9 3 Cyclopentanol, 3-methyl- 100 C6H120 018729-48-1 9 4 1,3-Butanediol, (S)-______________ 90 C4H10O2 024621-61-2 9 Abundance 7 Scan 90 (5.664 min): 26392.0 (-) m/z 41.00 100.00% 41 57 85 5000 72 X —I TTTTTTTTT T TTTTTTT 1 A 5.40 5.60 5.80 6.00 TIf TTI4 ■ I' ■ ' 1 11 T-r-j-, 111111111′12*111111 m/z 43.05 80.96% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #62509:1-Propene, 3-methoxy- 41 72

5000 "B I I I tiB )F TIT 1 * J | i t ( j j : J - F 5.40 5.60 5.80 6.00 57 m/z 45.00 79.01% 27 15 __ T I J____ _______ 12/22 I I 1*188 ‘ I ? । ■ I ■ ■ l • • » ■ 1 1BTT J J !if 1BB-m 1BI8 i : i j k mlz-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #2932: 2-Propen-1-ol, 2-methyl-, acetate 43 1* — I- 5.40 5.60 5.80 6.00 5000 m/z 57.10 70.87% 72

15 27 57 1_______ 1_______ I, - 114 • T i» ‘ 1 < । > । • • । • 1 ‘ * i ’ 1n1/" * ‘ H ’ ‘ ' 11111111111 T miz-> 10 20 30 40 SO 60 70 80 90 100 110 120 Abundance #1508: Cyclopentanol, 3-methyl- 57 5.40 5.60 5.80 6.00 71 m/z 85.00 55.44% 5000- 27 44 I 98 A TTI r r-t-i-j i i i11 ; ( T 1111 EUTT I ' ‘ ‘ ■ I 1 ‘ i ' 1 ‘ 1 i ' * ‘ 1 i • ‘ ■ i 1 m/z—> 10 20 30 40 50 60 70 90 100 110 120 5.40 5.60 5.80 6.00

26392.D NP112701.M Tue Dec 04 10:43:10 2001 Page 4

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