GCMS analysis results for sample AD26202, Dec 2001

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26203 .D vial: 26 Acq On : 1 Dec 2001 10:56 am Operator: GALOS Sample : gc/ms unknown 11/3 reext Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C: \DATABASE\NBS75K . L *************************************************************** *** *** Peak Number 5 1-Propen-2-ol, acetate Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 10.32 0.43 ng/uL 129940 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 entative ID MW MolForm CAS# Qual 1 1-Propen-2-o1, acetate 100 C5H802 000108-22-5 10 2 Pyrrolidine, 3-methyl- 85 C5H11N 034375-89-8 9 3 Oxepane, 2,2,4-trimethyl- 100 C6H120 023120-44-7 9 4 Hexane,/2-methyl- 100 C7H16 000591-76-4 9 Abundance Scan 597 (10.320 min): 26203.D (-) m/z 43.05 100.00% 1 43

5000- 59

' : 73 85 —PMAsa 10.00 10.20 10.40 10.60 5 ■ 1 117T > p ,, । p > 4 - । ■ l — L ' ' I ' 111 ‘ | ' 1 100 1 I ' 1 m/z 59.10 42.28% miz->_______1& 20___ 30 40 50 60 70 80 90 100 Abundance #63327: 1-Propen-2-ol, acetate 43

5000 | 10.00 10.20 10.40 10.60 ' 15 m/z 55.10 40.62% 58 j 27 ------- miz->_______10 20 +30 1 • 38 ! 1.... - 40 . .... 50 160.... 7270 — 80 90 100 100 Abundance #637: Pyrrolidine, 3-methyl- 43 -r-r-p-r-r-r-p-r AM--- - 10.00 10.20 10.40 10.60 5000 m/z 57.10 39.33% 85

, 157 56 68 —l...... - A 1 — ip, miz-> 10 20 30 40 50 60 70 80 90 100 Abundance #1525 Oxepane, 2,2,4-trimethyl- -m-p-T ' 111 1 1 ‘ I 43 10.00 10.20 10.40 10.60 59 m/z 41.10 35.26% 5000 1

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m/z—> TIT 10 31 TT ITIeum " 20 30 40 50 l— TPTT 85Tet 100 60 70 TT 80 90 100 AAA— ‘A1 A-12111 10.00 10.20 10.40 10.60 —M—

26203.D NP112701.M Wed Dec 05 10:42:49 2001 Page 5

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