GCMS Analysis Report for Sample AD26389, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26389.D Vial: 6 Acq On : 30 Nov 2001 4:46 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Oxepane, 2,2,4-trimethyl- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 5.22 1.74 ng/uL 741706 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Oxepane, 2,2,4- trimethyl - 100 C6H120 023120-44-7 64 2 Pentane, 2,4- dimethyl- 100 C7H16 000108-08-7 38 3 Pentane, 2,3- dimethyl- 100 C7H16 000565-59-3 35 4 Pentane, 2,3-dimethyl-__________ 100 C7H16 000565-59-3 35 Abundance ’ 7 Scan 41 (5.216 min): 26389.D () m/z 41.05 100.00% 4 56

5000 71. III: TT ( । i r T r । t i | i t 5.00 5.20 5.40 5.60

miz—> mmmmmmmmm m +51+ Hpmmm 100 TWTUITTTTTUTTTTTUIUI] 5 10 15 20253035404550 55 6065 70 7580859095 100105 m/z 56.10 75.56% Abundance #1525: Oxepane, 2,2,4-trimethyl- 43 59

5000 — TIBT —11 5.00 5.20 5.40 5.60 m/z 59.10 74.54%

1 31 85 100 TTWT Immp + Uuggug m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #1594: Pentane, 2,4-dimethyl- 43 57 < ■ i * • ■ ■ • i ■ ■

5.00 5.20 5.40 5.60 5000 m/z 43.10 69.93%

A 27 85

m/z—> mm 111‘" 'I 69 1 T—g—dmTnpu WpT 100 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63429: Pentane, 2,3-dimethyl- 43 55 5.00 5.20 5.40 5.60 m/z 42.05 58.85% 5000

miz—> 15 29

mm I"11!1 1111111111 TTmudi 71

85 I—TTITTT"’I 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 100 ■ ■

5.00 i ■ ■ L 5.20 5.40 5.60

26389.D NP112701.M Tue Dec 04 10:41:05 2001 Page 3

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