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GCMS Analysis Report for Sample AD26390, Dec 2001

Machine-extracted title · confidence 100%

Laboratory comment confirming detection of Butylbenzylphthalate in sample AD26390 on December 10, 2001.

NYC-WTC_000031491–000031508

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26390.D Vial: 4 Acq On : 30 Nov 2001 2:57 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Oxepane, 2,2,3-trimethyl- Concentration Rank 6 R.T. EstConc Area Relative to ISTD‘ R.T. 5.15 0.98 ng/uL 421361 1,4-Dichlorobenzene-d4 11.89 Hit# Of 5 entative ID MW MolForm CAS# Qual 1 Oxepane, /2,2,3 - trimethyl - 100 C6H120 023120-43-6 38 2 1-Pentanol, 4-methyl- 102 C6H140 000626-89-1 28 3 1-Hex me 84 C6H12 000592-41-6 25 4 Oxepa e, 2,2,4-trimethyl- 100 C6H120 023120-44-7 25 Abundance Scan 34 (5.154 min): 26390.D (-) m/z 41.05 100.00% 56

5000

71 ■ 1 1 i ' 1 1 1 1 1 1 1 1 i 1 67 | 50 1 5.00 5.20 5.40 5.60 m..... 37 HH TTp TE—Egg + 100 m/z 56.10 87.01%

1 mlz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1518: Oxepane, 2,2,3-trimethyl- 53

42 5000 T1mT 70 5.00 5.20 5.40 5.60 m/z 59.10 79.26% 27 mH Tpp53 H HTuttmunmnoauu ,85______ 100 ——299"B01133] miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63578: 1-Pentanol, 4-methyl- 56 41 69 5.00 ' 5.20 ' 5.40 ' ' 5.60 5000 m/z 42.05 66.52%

60 45 84 rrrTTTTpi , ’$’’—1’1111 pm “I"'11‘" Y •111 ’ “ TIUHTuga] mz—> 20 25 3035404550556065 70 75 80859095 100 105 Abundance #62755: 1-Hexene 41 56 5.00 1520 15.40 5.60 27 m/z 43.05 63.90% 5000 / 84 69 Tymgort T 51 mH ppupg rrrp-rr rnfz-> 2025303540455055 60 65 70 75 80 85 90 95 100105 5.00 ' 5.20 5.40 ' 5.60

26390.D NP112701.M Tue Dec 04 10:41:42 2001 Page 2

NYC-WTC_000031500

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NYC-WTC_000031500Source: NYC Law Department, mirrored locally

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