GCMS Analysis Report for Sample AD26390, Dec 2001

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26390.D vial: 4 Acq On : 30 Nov 2001 2:57 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208' 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 5.04 0.45 ng/uL 194377 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclohexane/ methyl- 98 C7H14 000108-87-2 91 2 2-Pentene* 3,4- dimethyl -, (Z)- 98 C7H14 004914-91-4 64 3 Cyclohexan e, methyl- 98 C7H14 000108-87-2 64 4 2-Pentene, 4,4- dimethyl -, (E) - Abundance C 98 C7H14 000690-08-4 53 Scan 22 (5.044 min): 26390.D (-) m/z ,83.05 100.00% 55 83

5000 41 98

70 4.90 5.00 5.10 5.20 5.30 5.40 5.50 ————1 + —H mH —54 H m/z 55.05 90.17% miz—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 7580 85 90 95100 105

A Abundance #1326: Cyclohexane, methyl- 83 55

5000 98 27 42 4.90 5.00 5.10 5.20 5.30 5.40 5.50 69 m/z 41.00 48.25% - mH H ' H ■ — 111111111 11 - 111111- + — n

m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63266: 2-Pentene, 3,4-dimethyl-, (Z)- 55 83 i ‘ * i" TTTOETTTTTTTT 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000 m/z ,98.05 42.01% 27 98

15 69 42 । -rm-p-rn- —————11117 TTPTTTTTTTTT TT’I ■n-p-r tmmp TWAr m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63234: Cyclohexane, methyl- 11 I 11 | H I , j .1 . . . |>* I“" I 55 83 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z 42.10 28.10% 5000 42 98 69 27

m/z—> ————1—— i > < i j: TT)’ tpor -Hmm +topmTT 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 11’111127 ITTTmTuf 4.90 5.00 5.10 5.20 5.30 5.40 5.50

26390.D NP112701.M Tue Dec 04 10:41:41 2001 Page 1

NYC-WTC_000031499