GCMS Analysis Report for Sample AD26389, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26389.D Vial: 6 Acq On : 30 NOV 2001 4:46 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise ! Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Propanoic acid, 2-methyl-, anh Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.14 1.18 ng/uL 502028 1,4-Dichlorobenzene-d4 11.89 Hit# of Tentative ID 5 MW MolForm CAS# Qual C. 1 Propanoic acia,2-metnyi-, anhydridM58 C8H1403 000097-72-3 59 2 Furan, 2-butyltetrahydro- 128 C8H160 001004-29-1 39 3 Furan, tetrahydro-2-(methoxymethyl) 116 C6H1202 019354-27-9 25 4 Cyclopentanol, 1-methyl - 100 C6H120 001462-03-9 9 Abundance Scan 142 (6.142 min): 26389.D (-) m/z 71.05 100.00% 71

5000 43 TI—ITIT ' 6.20 ’ TT TTTT Rd 57 5.80 6.00 6.40

miz-> ----- 20 30 40 —5150 60 I , —mmmmm 70 80 90 100 100 110 ' ■ i ■ ■ ■111 ■ 120 130 m/z 43.05 38.92% Abundance #11901: Propanoic acid, 2-methyl-, anhydride 71

43 5000 < i | i i : i | i T

5.80 6.00 6.20 6.40 m/z 41.0,5 22.83% 27

mlz-> 20 H 3744 30 40 55 —1—221— 1 • ‘ । ■ ■ ■ ■ i ■ ■ ■ ■ । 50 60 70 80 90 100 110 120 130 Abundance #5023: Furan, 2-butyltetrahydro- 71

5.80 6.00 6.20 6.40 1 5000 m/z 42.10 18.08% 27 42 55 mz-> -PH 20 30 40 ......... — 50 60 1 70 80 90 100 110 120 128 130 Abundance #3276: Furan, tetrahydro-2-(methoxymethyI)- IMfr ITT ' i ' * * * i 71 5.80 6.00 6.20 6.40 43 m/z 39.00 9.93% 5000

m/z—> 27 | • j ■ * • ■ j • ■ ■ • । ■ 20 30 40 58 + 1 1 i T‘‘r 1 i ‘ • 50 60 I,................ ....................... 116.................. 70 80 90 100 110 120 130 MRM 5.80 6.00 6.20 6.40

26389.D NP112701.M Tue Dec 04 10:41:05 2001 Page 4

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