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GCMS analysis results for sample AD26829, Dec 10 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26829 identifying unknown compounds on December 10, 2001.

NYC-WTC_000032202–000032222

Folder label: “GCMS X 11/7/01 A 12/6/01

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Scanned page image, NYC-WTC_000032213
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26829.D Vial: 6 Acq On 6 Dec 2001 2:44 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Propanoic acid, 2-methyl-, anh Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

6.12 1.79 ng/uL 516307 1,4-Dichlorobenzene-d4 11.89

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Propanoic acid, 2-methyl-, anhydrid 158 C8H14O3 000097-72-3 53 2 2-Hepten-3/ol, 4,5-dimethyl- 142 C9H180 055956-37-1 39 3 Furan, 2-butyltetrahydro- 128 C8H160 001004-29-1 38 4 Cyclopentanol, l-methyl- 100 C6H120 _______ 001462-03-9 33 Abundance Scan 140 (6.123 min): 26829.D (-) m/z 71-05 100.00% 71

5000 43

55 5.80 6.00 6.20 6.40______ m/z-> 10 20 30 37140 - —l1 50 60 70I 80 90 100 110 100 120 130 m/ z 43.05 45.62% Abundance #11901: Propanoic acid. 2-methyl-, anhydride 71

43 ' • I < > • ' I ' 1 ' ' I 5000 5.80 6.00 6.20 6.40 m/z 24.40% 371 , 27——— 55........................................................................................ 41.10 miz-> Abundance

5000 10 20 30 40

43 50 60 70 80 90 #8051: 2-Hepten-3-ol, 4,5-dimethyl- 71 100 110 120 130

W m/ z 5.80 ----4 TTT 6.00 42.10 6.20 6.40 21.43% 27 15 I 55 TPTmB——m—t0md/1n//—/0//—/oB00—B/Bn/—om 81 100 109 124

m/z-> 10 20 30 40__ 50__ 60___ 70 80 90 100 110 120 130 i Abundance #5023: Furan, 2-butyltetrahydro- 71 ___ 5.80 A O' TT 6.00 6.20 6.40______ m/z 39.00 10.39% 5000-

27

i ' i ■ ' ' i ' ’ ' ■ i ■ 42 -HP TTT —T 55 ' I ‘ ' i ' ' ' ' I ' ' 1 ' ! ' ' ' TIOuIIIut 128 ............AAA ‘ . I . . . . I TT. . I r r .■, I ,■ . , T I m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 5.80 6.00 6.20 6.40

26829.D NP112701.M Fri Dec 07 14:54:31 2001 Page 5

NYC-WTC_000032213

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NYC-WTC_000032213Source: NYC Law Department, mirrored locally

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