GCMS non-target scan comment, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26203.D Vial: 26 Acq On : 1 Dec 2001 10:56 am Operator: GALOS Sample : gc/ms unknown 11/3 reext Inst : GC/MS Ins Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 1-Propen-2-ol, acetate Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 10.32 0.43 ng/uL 129940 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Propen-2-ol, acetate 100 C5H802 000108-22-5 10 2 Pyrrolidine, 3-methyl- 85 C5H11N 034375-89-8 9 3 Oxepane, 2,2,4 - trimethyl- 100 C6H120 023120-44-7 9 4 Hexane, 2-methyl- 100 C7H16 000591-76-4 9 Abundance Scan 597 (10,320 min): 26203.D(-) m/z 43.05 100.00% 43

5000

y 73 85 “TMen — — - - 10.00 10,20 10,40 10,60 ------+ + - - , — — 190 m/z 59.10 42.28% miz-> 1 20 30 40 60 70 80 90 100 Abundance #63327: 1-Propen-2-ol, acetate 43

5000 T T 1’I T T 10.00 10.20 10.40 10.60 15 58 m/z 55.10 40.62% .— 38 1 —.. — 72 190 • 1 • • • • 1 ■ • ■ • ] t • • i mfe-> 10 20 30 40 50 60 80 90 100 Abundance #637: Pyrrolidine, 3-methyl- 43 _— L A 10.00 10.20 10.40 10.60 5000 m/z 57.10 39.33% 85 15 -- 27 56 68 mlz-> Abundance 10 20 30 40 50 —t m 1 1 1 60 70 #1525: Oxepane, 2,2,4-trimethyl- 43 59 80 1 "I" I I I I I 1 90 100 1-111 N * ‘I ‘ ‘ ‘ 1 1 10.00 10.20 10.40 10.60 m/z 41.1.0 35.26% 5000

31 • ■ I ‘ 1 ' ‘ I ' 1 1 ■ l'1 1 ■ ' i ' , 41 JI.. T 85 100 1T 11TT P . —11 AAA _ L J, M * ‘ ‘ I miz—> 10 20 30 40 50 60 70 80 90 100 10.00 10.20 10.40 10.60

26203.D NP112701.M Tue Dec 04 15:06:01 2001 Page 5

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