GCMS Analysis Report for Sample AD26390, Dec 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26390.D vial: 4 Acq On : 30 Nov 2001 2:57 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hepten-3-ol, 4,5-dimethyl- Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.14 1.07 ng/uL 462041 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual ( 1 2-Hepten-3-ol, 4,5-dimethyl- 142 C9H180 055956-37-1 40 2 Cyclopentanol, 1-methyl- 100 C6H120 001462-03-9 36 3 Cyclopentanol, 1-methyl- 100 C6H120 001462-03-9 9 4 Propanoic acid, 2-methyl-, anhydrid 158 C8H14O3 000097-72-3 9 Abundance Scan 142 (6.144 min): 26390.D (-) m/z 71.05 100.00% 71

5000 43

55 ' ' 5.80 6W ‘ ] 6.20 ‘ 6.40 ‘ • T -— 100 — TIuu:uungun,ogr m/z 43.05 41.33% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #8051: 2-Hepten-3-ol, 4,5-dimethyl-

A 71

5000 43 1 ‘ I 1 ‘ ‘ ' I ' ' ‘ I ' ‘ ' I ' ' 1 ' I ' 5.80 6.00 6.20 6.40 27 m/z 41.05 20.76% 55 N 15 11 , 81 100 109 124 1/1/1/1/11/211111/7*11r/61 ‘‘8 11 — TIn—Bdur ■ i ' • ■ ■ i ' ■ ' • i • miz—> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #63340: Cyclopentanol, 1-methyl-

43 71 58 5.80 6.00 6.20 6.40 IT 5000 m/z 42.10 18.43% 85

m/z-> 10 ....... I, 51, 20 30 40 50 60 I ‘ ‘ ’* I 70 80 A 90 100 ।। 100 p 11.1111111 110 120 130 Abundance #1511: Cyclopentanol, 1-methyl- —AIAIAI T 71 5.80 6.00 6.20 6.40 m/z 39.00 10.61% 43 5000 58

27 85 15 | 111/11/1/11/"1/1//1/1//71/1/1"1/6/0/L71 100 i1 — H 1' ■ [ ■>■■■ 1 13 । n. ■ » « I » » » ‘ I ’ M ., , 4 .1 A A AA m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 5.80 6.00 6.20 6.40 ' ‘'

26390.D NP112701.M Tue Dec 04 10:41:43 2001 Page 4

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