GCMS Analysis Report for Sample AD26390, Dec 2001

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Laboratory comment confirming detection of Butylbenzylphthalate in sample AD26390 on December 10, 2001.

NYC-WTC_000031491–000031508

Folder label: “GCMS X 11/5/01 A 12/1/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26390.D Vial: 4 Acq On : 30 NOV 2001 2:57 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Butanol, 3-methyl-, (S)- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.19 3.88 ng/uL 1675080 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 ntative ID MW MolForm CAS# Qual 1 2-Butanol,/3-methyl-, (S)- 88 C5H120 001517-66-4 38 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 2-Butanol, 3-methyl- 88 C5H120 000598-75-4 9 4 2-Butanol, 3-methyl- 88 C5H120 000598-75-4 9 Abundance Scan 256 (7.189 min): 26390. D (-) m/z 45.10 100.00% 45

5000 61 73 1 * ■ ।11 I D —P 6.80 7.00 7*20 7.40 7.60 mmmmmmlt " | ITT!91 |‘l H 111 । ■ 111... ।|.i ■ <111 ■ ■ 11111111> 207 m/z 43.00 57.39% miz-> 10 2030405060 70 8090 100110120130140150160170180190200210 Abundance #852:2-Butanol, 3-methyl-, (S)- 45

5000 T TIT rT | 'i i ; , । , i । । । r i tt । .T 6.80 7.00 7.20 7.40 7.60 m/z 73.05 38.61% 27 55 73 mmpm L ...... 41418 ,1..... 87.................................... 11>।.IT.. 111.11.,,. ।.... ।....।.... ।,.,. ।..., ।, miz-> 10 2030405060 70 8090 100110120130140150160170180190200210 Abundance #292: N-Ethylformamide 33 73 6.80 7.00 7.20 7.40 7.60 5000- m/z 61.00 38.12% 44 58

15 miz-> mp m.. TTUmpp 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #62962:2-Butanol, 3-methyl- ‘ I 1 ‘ ‘ i 1 ‘ r ‘ I 1 ‘ ‘ I 1 ‘ ‘ ' 1 1 1 45 6.80 7.00 7.20 7.40 7.60 m/z 44.00 10.60% 5000

27 55 73 ii. ■. I . . . . | 1 . I . ... 88| .... | .... I 11 11 j ,, .. | . . . . | . . . . | I H , |. H . | . I 11 | I I I I | I I I I |! I | ( U -r-ri 111 i111 11 111 ' i'1 1 11 11 m/z—> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 6.80 7.00 7.20 7.40 7.60

26390.D NP112701.M Tue Dec 04 10:41:44 2001 Page 5

NYC-WTC_000031503

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GCMS analysis report for sample AD26392, Dec 2001 · Box DEP Box 21

NYC-WTC_000031530

DEP lab report dated December 4, 2001, documenting GCMS analysis of sample AD26392 noting other unknown compounds.

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